GCMS analysis results for sample AD26711, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26711.D Vial: 5 Acq On 5 Dec 2001 12:24 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Ethane, 1,1,2,2-tetrachloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.61 0.68 ng/uL 239955 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 2 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 93 3 Ethane, 1,1,2-trichloro-2-fluoro- 150 C2H2C13F 000359-28-4 72 4 Ethane, 1,2,2-trichloro-1,1-difluor 168 C2HC13F2 0 0354-21-2 43 'Abundance Scan 520 (9.608 min): 26711 .D (-) m/z 82.9 100.00% 83

5000

47 61 133 168 9.20 ' ' 3.2079.60/73.80 ' 10.00” 37 i ■ ■ । ■ ■ • ■ ।1 ----- Tr"111 4 1TTIIT - m/z 84.95 70.32% m/z~> 30 40 50 60 . 70 80 90 100 110 120 130 140 150 160 170 Abundance #67919: Ethane, 1,1,2,2-tetrachloro- 83

5000- 9.20 9.40 9.60 9.80 10.00 j 35 m/z 94.95 14.34% 60 96 ; m/z-> 30 447, 40 50 60 70 -mmmPP 131 11 ‘I’’ 80 90 100 110 120 130 140 150 160 170 I ■- 168

Abundance #13774: Ethane. 1,1,2,2-tetrachloro- 83

9.20 9.40 9.60 9.80 10.00 5000- m/z 61.00 11.10%

95 131 168 35 47 I TTTTT l • • ■ ■ । ■. • • । • I > ■ TTTT P TT’TTT T-p-t । • ■ • • । ■ ■ • • । — m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #9542: Ethane, 1,1,2-trichloro-2-fluoro- i 83 9.20 9.40 9.60 9.80 10.00 m/z 96.95 10.85% 5000 67 35 47 95 150 — m TPPTE ITT l , 11 -----PPP 1 111 11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 9.20 9.40 9.60 9.80 10.00

26711.D NP112701.M Fri Dec 07 13:14:36 2001 Page 4

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