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GCMS calibration table, Dec 2001

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Calibration data table for gas chromatography-mass spectrometry analysis dated December 3, 2001.

NYC-WTC_000031350–000031358

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C: \HPCHEM\1\DATA\NOV3 0 01\LBA. D Vial: 15 Acq On 1 Dec 2001 12:56 am Operator: GALOS Sample lb 11/5 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 4.943 6 11 15 rBV 57640 107694 1.50% 0.292% 2 5.007 15 18 24 rVB 51990 81351 1.13% 0.220% 3 5.163 32 35 44 rW2 22958 72278 1.00% 0.196% 4 6.107 133 138 145 rBV 17176 74649 1.04% 0.202% 5 6.566 184 188 193 rBV 37529 77609 1.08% 0.210% 6 7.171 249 254 267 rBV 114742 267343 3.71% 0.724% 7 7.850 324 328 346 rVB 581972 1402769 19.47% 3.798% 8 10.326 593 598 608 rBV 68571 147498 2.05% 0.399% 9 10.537 617 621 629 rVB 54186 106813 1.48% 0.289% 10 11.894 763 769 787 rBV 2651616 5714404 79.33% 15.472% 11 15.507 1157 1163 1181 rBV 3469188 7203074 100.00% 19.503% 12 20.780 1732 1738 1749 rBV 3331525 7055764 97.95% 19.104% 13 25.181 2212 2218 2230 rBV2 2865994 6342620 88.05% 17.173% 14 25.328 2230 2234 2241 rVB2 25923 73372 1.02% 0.199% 15 33.187 3085 3091 3106 rBV2 2054528 4475236 62.13% 12.117% 16 37.277 3529 3537 3550 rBV2 1366037 3658208 50.79% 9.905% 17 41.220 3966 3967 3969 rBV 126146 73144 1.02% 0.198%

Sum of corrected areas: 36933826 LBA.D NP112701.M Tue Dec 04 10:14:02 2001

NYC-WTC_000031354

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NYC-WTC_000031354Source: NYC Law Department, mirrored locally

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