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GCMS calibration table for TCLP analysis, Dec 2001

Machine-extracted title · confidence 100%

Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.

NYC-WTC_000031876–000031888

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DECO6O1\LBA.D Vial: 10 Acq On 6 Dec 2001 6:23 pm Operator: GALOS .Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.069 21 25 38 rBV 678534 1732862 27.89% 4.568% 2 6.132 137 141 147 rBV3 21103 73390 1.18% 0.193% 3 6.490 177 180 188 rBV3 31135 101651 1.64% 0.268% 4 6.600 188 192 201 rW 35688 96305 1.55% 0.254% 5 6.719 201 205 214 rW 43974 158984 2:56% 0.419%

6 6.839 214 218 226 rVB2 31501 92560 1.49% 0.244% 7 7.205 253 258 276 rW 1526241 2874872 46.27% 7.578% 8 7.875 327 331 346 rBV 879662 2053541 33.05% 5.413% 9 9.388 491 496 504 rBV 61322 125256 2.02% 0.330% 10 9.635 518 523 537 rVB2 213450 740203 11.91% 1.951%

11 10.332 595 599 606 rVB 45746 94811 1.53% 0.250% 12 10.543 618 622 630 rBV 39868 86802 1.40% 0.229% 13 11.891 764 769 785 rBV 2413277 5107713 82.20% 13.464% 14 14.514 1051 1055 1059 rVB 46869 88033 1.42% 0.232% 15 15.504 1157 1163 1183 rBV 3025708 6213579 100.00% 16.380%

16 20.777 1732 1738 1753 rBV 2828564 6105310 98.26% 16.094% 17 25.179 2212 2218 2232 rBV2 2414647 5445636 87.64% 14.355% 18 33.184 3085 3091 3109 rBV2 1719405 3897855 62.73% 10.275% 19 33.450 3115 3120 3127 rVB 27425 66419 1.07% 0.175% 20 37.274 3530 3537 3559 rBV2 996493 2778907 44.72% ♦ 7.326%

Sum of corrected areas: 37934689

LBA.D NP112701.M Wed Dec 19 13:08:40 2001

NYC-WTC_000031880

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NYC-WTC_000031880Source: NYC Law Department, mirrored locally

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