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GCMS calibration table for TCLP analysis, Dec 2001

Machine-extracted title · confidence 100%

Calibration data sheet for GCMS analysis using TCLP method, listing standards and response factors from December 2001.

NYC-WTC_000032693–000032700

Folder label: “GCMS X 11/13/01 A 12/8/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\DEC0701\LBB.D Vial: 12 Acq On 8 Dec 2001 4:08 am Operator: GALOS Sample gc/ms unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.041 16 22 30 rVB 44401 87001 1.13% 0.219% 2 6.480 174 179 186 rBV 40568 77713 1.01% 0.196% 3 6.581 186 190 194 rBV 50387 102063 1.32% 0.257% 4 6.829 213 217 225 rBV 34675 79930 1.04% 0.202% 5 7.847 324 328 343 rVB 587893 1235071 16.00% 3.114%

6 11.872 761 767 790 rBV 2896029 5894578 76.38% 14.864% 7 15.486 1154 1161 1178 rBV 3315279 7421822 96.17% 18.715% 8 20.758 1729 1736 1758 rBV 3758713 7717247 100.00% 19.460% 9 25.169 2211 2217 2229 rBV2 3319019 7116833 92.22% 17.946% 10 25.316 2229 2233 2243 rVB 27743 84027 1.09% 0.212%

11 33.175 3084 3090 3110 rBV2 2408175 5428949 70.35% 13.690% 12 37.264 3527 3536 3562 rBV2 1624510 4411329 57.16% 11.124%

Sum of corrected areas: 39656563

LBB.D NP112701.M Tue Dec 11 15:14:18 2001

NYC-WTC_000032697

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NYC-WTC_000032697Source: NYC Law Department, mirrored locally

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