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GCMS calibration table for TCLP analysis, Dec 6 2001

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Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 6, 2001.

NYC-WTC_000032269–000032285

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.045 15 22 28 rBV 91987 177088 1.90% 0.354% 2 5.155 30 34 37 rW 198457 330059 3.53% 0.659% 3 5.210 37 40 56 rVB 268307 572320 6.12% 1.143% 4 6.136 137 141 155 rBV 166966 366317 3.92% 0.732% 5 6.485 175 179 187 rBV 86186 170042 1.82% 0.340%

6 6.595 187 191 201 rW 81189 186218 1.99% 0.372% 7 6.723 201 205 213 rVB 50216 109662 1.17% 0.219% 8 6.833 213 217 228 rBV2 47930 122294 1.31% 0.244% 9 7.182 248 255 263 rBV 220954 504398 5.40% 1.008% 10 7.860 325 329 341 rBV 392100 821835 8.79% 1.642%

11 10.318 592 597 605 rBV 204683 391770 4.19% 0.783% 12 10.529 614 620 630 rBV 100164 199001 2.13% 0.398% 13 11.886 763 768 785 rVB 3674771 7422712 79.43% 14.828% 14 15.499 1155 1162 1181 rBV 4420310 9344433 100.00% 18.667% 15 20.772 1731 1737 1754 rBV 4470753 9231935 98.80% 18.442%

16 25.183 2212 2218 2230 rBV2 4045922 8568909 91.70% 17.118% 17 33.188 3084 3091 3108 rBV2 2817559 6353289 67.99% 12.692% 18 37.278 3529 3537 3554 rBV2 1889581 5187027 55.51% 10.362%

Sum of corrected areas: 50059309

LBB.D NP112701.M Wed Dec 12 08:18:53 2001

NYC-WTC_000032273

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