GCMS analysis page for sample AE11572, May 2002

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Data File : C:\MSDCHEM\1\DATA\020521\11572 .D Vial: 25 Acq On : 22 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Propenal, 3-(3,4-dimethox... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.33 ug/1 32154 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propenal, 3-(3,4-dimethoxyphen. . . 192 C11H1203 004497-40-9 53 2 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 47 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 47 4 3-(2/-Methoxy-5-methylphenyl ) acry. . . 192 C11H1203 103986-76-1 43 Abundance Scan 4768 (31.094 min): 11572.D (-4758) (-) m/z 192.10 100.00% 192

5000 96 40 49 146 160 106 118. mm 66 86 30.80 31.00 31.20 31.40

m/z-> 0 -H .... .................... -H 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/ Z 96.00 22.23% Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 11 1...... 5000 ' T 1 ' 1 1 I 11 'I ' ' ' 1 1 1 ' 30.80 31.00 31.20 31.40 77 121 149 177 m/z 191.10 19.92% 91 103 52 64 138 0 ' 11' " I " " 111" 1l 111 i'l I' ।' । ■ > ..... I i * *■ ‘I’ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192 ,I.... .......... 30.80 31.00 31.20 31.40 5000 m/z 160.10 13.95% 175 63 89 11 145 45 .1 77 | 105 117 0 TTTH++H#Tr’tpi’t’t’i । Itst’i 111 I’I’ ) 11 r’r]" 111 |‘‘l 1111’ltt 1111111 135 | 163 tmmmn mz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 4 30.80 31.00 31.20 31.40 m/z 193.20 13.92% 5000

„ 96 165

n/z-> 29 39 51 63 74 83 i 115 126 139 152 , 176 0 ‘ITua’uut T1‘ 11 j I'i 11 j । i'i i 1) 1 i'l i jTi i'1'i i Pl 1111 1111 ri j |-j 11 ip 111'| 1111 pi 1111 iTi 111 rh I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Lp ' 1 i 1 ■ ■ 1 i ' ' 30.80 31.00 31.20 31.40 1 1 i ■ ■

11572.D SCAN020521.M Fri May 24 09:51:53 2002 Page 5

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