GCMS analysis report for sample AE11572 showing unknown compounds and surrogate recovery data from May 29, 2002.
NYC-WTC_000025624–000025634Folder label: “GCMS X 5/17/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LDLaLy oearcI compouru Kepor L
Data File : C:\MSDCHEM\1\DATA\020521\11572.D Vial: 25 Acq On : 22 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 *************************************** * * **************************** Peak Number 4 Quinazoline, 4-(1-methyleth... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.40 ug/1 38491 Phenanthrene-dl0 31.72 Hit# of Tentative ID MW MolForm CAS# Qual
1 Quinazoline, 4-(1-methylethyl). 188 C11H12N2O 050915-32-7 33 2 2,6-Naphthoquinone , 1,5-diamino- 188 C10H8N2O2 002783-59-7 33 "A Anthracene-dlO- 4 Phe nthrene-dlO Abundance Scan 4915 (31.958 min): 11572. D (-4907) (-) 188 188 C14D10 C14D10 m/z 188.20 001719-06-8 001517-22-2 100.00% 23 23 188
5000 94 /................ 66 160 44 31.60 31.80 32.00 32.20
m/z-> 0 20 —l 40 60 —IWWIIPIOTTPIWIWTTTTTT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 340 m/ z 94.10 39.57% Abundance #79808: Quinazoline, 4-(1 -methylethyl)-, 1 -oxide 188 , I / . - -I t I I I ... I . 173 5000 31.60 31.80 32.00 32.20 157 m/Z 160.10 22.60% 1 115131
z-> O-ni ■ . .. 71—tl 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 '' I " " I ■ " • I' ‘ " I'1'11 “ " I ' " 11" 11"
Abundance #79755:2,6-Naphthoquinone, 1,5-diamino- 188 31.60 31.80 32.00 32.20 132 m/z . 65.90 19.81% 5000 160
66 104
0 ----rh+89—4 4' r TTTTT 28 51 I I "II" i ________ ' ■ i " " i ■ " ■ i' I ■1' ■ i1' n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79826: Anthracene-d10- ■ rr ‘ r TIIIIIgu 188 31,60 31.80 32.00 32.20 m/z 189.20 19.28% 5000
94 160 , 17 42 66 ....... .. I'll ’ 1’111111211010111101—001000100711" 0 1-rp ri । |'i i l'i 1’ i nz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31,60 31.80 32.00 32.20
11572.D SCAN020521.M Fri May 24 09:51:53 2002 Page 6
NYC-WTC_000025633
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NYC-WTC_000022550
Laboratory report of GCMS analysis for sample AE11427 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024935
Chromatogram and integration data from Method 508 GC/MS analysis of sample AE10302 performed on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022598
Laboratory report of GCMS analysis for sample AE11566 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025603
GCMS analysis report for sample AE11570 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024613
Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024575
Laboratory report documenting GCMS analysis of sample AE11285 conducted on May 28, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022516
Reference standard analysis report for nitrosamines and benzene derivatives in sample AE11424 analyzed May 17-21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024380
Chain of custody record for GCMS analysis of sample AE10237 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024681
Laboratory report documenting GCMS analysis of sample AE11159 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046203
Laboratory report documenting GCMS analysis of sample AE10136 conducted on May 17, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000025494
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025495
Laboratory log sheet recording Method 608 extraction parameters and sample counts for sample AE11423 in May 2002.
Filed in the same folder
NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025508
Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025512
Laboratory report of GCMS reference standard analysis showing response values for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder