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GCMS analysis page for sample AE11572, May 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE11572 showing unknown compounds and surrogate recovery data from May 29, 2002.

NYC-WTC_000025624–000025634

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025631
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NYC 9/11 Public Portal Document Llbrary searen Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11572 .D Vial: 25 Acq On : 22 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Benzene, l-chloro-3-(trichl... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.20 ug/1 19471 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, l-chloro-3-(trichloroet... 240 C8H4C14 000704-21-2 32 2 9,10-. thracenedione, 1-chloro- 242 C14H7C1O2 000082-44-0 9 3 [4-(4 Methoxymethylbenzyl)phenyl... 242 C16H18O2 1000202-05-8 9 4 Uraci , 1,3-dimethyl-6-trimethyl... 242 C10H18N2O3Si 1000153-43-2 9 Abundance Scan 4395 (28.902 min): 11572.D (-4387) (-) m/z 241.90 100.00% 24,2

207 5000 40 55 73 85 o- 3. 111 136 172 229 ....0... ... m/z—> 0-P 20 40 ■ Ii ■ '

60 i ■ ■ ' '

80 i

100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20 m/z 206.95 49.22% Abundance #91662: Benzene, 1-chloro-3-(trichloroethenyl)- 242

... 5000 170 ■ ' i ' 1

139 28.60 28.80 29.00 29.20 36 50 . 74 99 111 207 m/z 172.00 43.97%

n/z-> O-T 20 Jpl4 40 60 80 1. .... 1,225 —ll— 240 100 120 140 160 180 200 220 Abundance #127435:9,10-Anthracenedione, 1-chloro- 2-2

214 28.60 28.80 29.00 29.20 5000 m/z 208.90 40.07% 186 75 151

27 39 50 62 ll , 93 110 125 139 . 164 m/z-> 0 Imnn/mm ’ I r r, "r i ’"r , , r. , . । , .1 TTT 20 40 60 80 100 120 140 160 180 200 -199 220 | 227 | L 240 Abundance #91638: [4-(4-Methoxymethylbenzyl)phenyl]methanol 2-2 28.60 28.80 29.00 29.20 107 m/z 244.00 36.72% 5000 136 165 211 79 91 179 118 152 31 43 57 , 197 9 bl, , * 1 | | lp Mlm .ill]! qin l ,, I, h —r 0 I ' 1 1 ' 1 1 1 1, । A , 4,, i. Tl 1—T ■ ■ i ■ • ■ ■ i ■ 1 ' i ■ ' ‘ |_r 1 1 1 ■ । /z—> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

11572.D SCAN020521.M Fri May 24 09:51:53 2002 Page 4

N YC-WTC_000025631

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NYC-WTC_000025631Source: NYC Law Department, mirrored locally

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