GCMS analysis results for sample AE11156, May 2002

NYC 9/11 Public Portal Document ULJL CL Y OCaL’ii COIpOULIU RCDOL L

Data File : C: \MSDCHEM\1\DATA\020515 11156 .D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Anthracene, 1-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.08 0.20 ug/1 22476 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 1-methyl- 192 C15H12 000610-48-0 59 2 Anthracene, 192 C15H12 2-methyl- 000613-12-7 59 3 Bitoscanate 192 C8H4N2S2 004044-65-9 59 4 Phenanthrene, 4-methyl-_________________ 192 C15H12 000832-64-4 59 Abundance Scan 4765 (31.076 min): 11156.D (-4751) (-) m/z 192.10 100.00% 192

5000

44 70 82 96 126 146 164 I 30.80 31.00 31.20 31.40 —TTHTHpmmmmmmmmmm "i" m/z 193.00 12.98% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150 160 170180190 200 Abundance #125854: Anthracene, 1-methyl- 192

5000 1 ■ i ■ 1 30.80 31.00 31.20 31.40 m/ Z 190.90 12.79% 82 94 165 18 27 39 51 63 | Il 115 126 139 150 | 176 „ ' । ■ ■ ■ 1111 i‘i । i 111'| 11: i |'i 11 j । Pi i 1111’l'i 111 l'l'| 111T r r i rI‘ i 111! 111 r n’j 111 r pl 111 [llrrte r i1 ! Tg miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #125844: Anthracene, 2-methyl- 192 ‘ I‘* ' 1 I 1 1 1 ‘ I ' 4 30.80 31.00 31.20 31.40 5000 m/z 82.20 11.44%

no 96 165 63 74 7 II 115 139 150 I 176 ' I " ' ' I " ' ' i 1 ' " I " " I " " I " " I " " I 11 ' 1 I ' 1 1 ' I " ' ' 1 1 1 " I । । । । I " । ''I 1 1 ' ' I । । । । | 1 1 1 । | । । I I | I ! l'!1 ‘ ‘I’’ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #80930: Bitoscanate 192 m/ z 96.00 9.61% 5000 134 90 160 50 63 75 /z-> 26 ' i" " i" " i1 TTT 39 10 20 30 40 50 60 70 80 90 100110120130140150 160 170 180190 200 । ,107116 148 ■ ' I l I1"1! | ■ I. ... .'I HH 1 F}Tm. ...... i]....... 30.80 31.00 31.20 31.40

11156.D SCAN020507.M Thu May 16 09:37:12 2002 Page 9

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