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GCMS analysis results for sample AE11156, May 2002

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Laboratory report documenting GCMS analysis of sample AE11156 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024514–000024528

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024525
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NYC 9/11 Public Portal Document j_ij.ijj.cixy sedrcI topounu KeporL

Data File : C:\MSDCHEM\1\DATA\020515\11156.D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

28.91 0.20 ug/1 22325 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 25 2 4-Bromo-2,6-difluoroaniline 207 C6H4BrF2N 067567-26-4 10 3 Quinoline, 8-bromo- 207 C9H6BrN 016567-18-3 10 4 Quinoline,3-bromo- 207 C9H6BrN 005332-24-1 9 Abundance/ Scan 4397 (28.914 min): 11156.D (-4385) (-) m/z 245.90 100.00% / 209 24/6

85 136 5000 99 174

—51 40 121 227 L 28.60 28.80 29.00 29.20 ’ I 1 1 i ■ ■ ■ ■ i ' 1 TOn"TI" ‘‘ 'T' 1 ■ ' | m/ Z 2 09.00 92.99% m/z-> Abundance 20 40 60 80 100 120 140 160 #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 180 200 207 220 240 I 244 5000 136 28.60 28.80 29.00 29.20 74 85 99 m/z 242.00 85.19% 51 63 171

m/z-> 20 Hls +,+,110′21,. 40 60 80 100 120 III , , 157 . , 193 , 140 160 180 200 229 i. +tt 220 240 Abundance #85328: 4-Bromo-2,6-difluoroaniline 209 1,... H......... 28.60 28.80 29.00 29.20 5000 128 m/ z 2 06.90 77.91% 108 81 — 31 +44457.88,83 1 ....... 160 179. , ————— L miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #84881: Quinoline, 8-bromo- II A 1 207 28.60 28.80 29.00 29.20 128 m/z 243.90 62.70% 5000 101 50 64 75 27 39 I -"pi "r ' . . "'I tt 9 ,41.117, ——142154 171 184 —————— h,. ........ nfz~> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

11156.D SCAN020507.M Thu May 16 09:37:10 2002 Page 8

NYC-WTC_000024525

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NYC-WTC_000024525Source: NYC Law Department, mirrored locally

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