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GCMS analysis results for sample AE11156, May 2002

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Laboratory report documenting GCMS analysis of sample AE11156 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024514–000024528

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024524
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NYC 9/11 Public Portal Document ULLDLCLX OEdLtii totpOuIU KCDOL L

Data File : C:\MSDCHEM\l\DATA\020515\11156.D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Benzene, trichloro-1,3-dime... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.30 0.22 ug/1 22815 Acenaphthene-dl0 24.46 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, trichloro-1,3-dimethyl- 208 C8H7C13 054965-20-7 15 2 2-Propenoic acid, 3-(dimethylami... 212 C11H20N2O2 049582-41-4 12 3 Isoquinoline-5-boric acid 173 C9H8BNO2 1000214-23-4 10 4 3-Chloro/4-nitrophenol 173 C6H4C1NO3 000491-11-2 9 Abundance Scan 3271 (22.298 min): 11156. D (-3260) (-) m/ z 210.00 100.00% 84 210 173

5000 138 k...... I)... 1 .268 ........ .... 546 ' ' i ' ■ ■ ■ i ' 1 51 22.00 22.20 22.40 22.60 m/ Z 83.90 90.27% iz—> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #75330: Benzene, trichloro-1,3-dimethyl- 173 208 ly 5000 22.00 22.20 22.40 22.60 68 102 137 m/z 173.00 83.85%

n/z-> 0 . .28, 4A44r 50 100 4 ul 150 200 250 300 350 400 450 500 550 Abundance #33832:2-Propenoic acid, 3-(dimethylamino)-3-(1 -piperidin... 84 114 — ., 1..... 1 1 ' I ’ 1 ’ 1 1 1 1 ' ' 1 1 ' 22.00 22.20 22.40 22.60 5000 42 m/z 174.90 39.03% 212 139 1/0 - TT n/z—> Abundance 0 50 100 150 200 250 300 350 #75220: Isoquinoline-5-boric acid 113 400 450 500 550 L 22.00 22.20 22.40 22.60 m/z 137.90 36.34% 5000 128 75 50 101

TT ., ul u i 1 . m/z— > 0 50 100 150 200 250 300 350 400 450 500 550 22.00 22.20 22.40 22.60

11156. D SCAN020507.M Thu May 16 09:37:09 2002 Page 7

NYC-WTC_000024524

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NYC-WTC_000024524Source: NYC Law Department, mirrored locally

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