GCMS analysis results for sample AE11156, May 2002

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Data File : C:\MSDCHEM\l\DATA\020515\11156.D Vial: 22 Acq On : 16 May 2002 8:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 8 Pentacyclo[7.3.1.1. (4,12) . 0 . . Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.34 ug/1 37301 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacyclo[7.3.1.1. (4,12) . 0 (2,7) ... 188 C14H20 1000215-61-8 47 2 Phenanthrene -diO 188 C14D10 001517-22-2 45 3 Pentacyclo[8.4.0.0 (3,7) .0 (4,14) . . . . 188 C14H20 1000099-27-2 37 . 4 Anthracene-d10- 188 C14D10 001719-06-8 33 Abundance Scan 4914 (31.952 min): 11156.D (-4905) (-) m/ z 188.20 100.00% 188

5000 80 .............. .......................................... 94 156 52 66 108 320 31,60 31.80 32.00 32.20

m/z-> T‘ 14 1,4 la. .... 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 1 ■ i ■'' ■ i1 ■ ■ ■ । '111' ■ ■ ■ ।1 ■'111 m/z80.10 42.00% Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)]tetradeca... 188

5000 91 7.’ 31.60 31.80 32.00 32.20 55 131 m/z 184.10 33.90% 105

1‛r , , 145159,73— hatiyahaaandi /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/ Z 94.10 23.26%

80 94 160 30 r ■ 1 ■ T' 52,66.4444,108 132146 ,|| ' I " " I ' '' i ■ ■ ■ ■ i ‘■ i ■ ■ ■ ■ i ■ ■ ■ ■ i' ‘'11' ■ i' ■ /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane 188 31.60 31.80 32.00 32.20 m/ z 92.20 22.44%

5000 91 117131145159173 41 7.’ .. — 1 .~ | I l I 1 | I !! I | I

m/z—> 27, 1 55 A, I,, 44 '' I'''111''' I ‘ 11' I 1''' I ’1'11'' *' 111 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 31.60 31.80 32.00 32.20

11156.D SCAN020507.M Thu May 16 09:37:16 2002 Page 10

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