GCMS chain of custody form, sample AE10986, May 2002

NYC 9/11 Public Portal Document LlDrary searcn compound Keport

Data File : C:\MSDCHEM\1\DATA\020515\10986.D Vial: 16 Acq On : 16 May 2002 2:37 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Methane, dibromochloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

5.08 0.60 ug/1 43987 1,4-Dichlorob'enzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 95 2 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 50 3 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 38 4 Methane, bromochloroiodo- 254 CHBrClI 034970-00-8 17 Abundance Scan 341 (5.083 min): 10986.D (-336) (-) m/z 128.90 100.00% 129

5000

49 1MMMA Pijii 79 91 35 .I — 160 210 259 4.80 5.00 5.20 5.40 mHH 11 1 1 1 ---------- m/z 126.90 70.78% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121838: Methane, dibromochloro- 129

5000 4.80 5.00 5.20 5.40 79 m/z 131.00 23.01% 48 13 2, 1..... , J|l,93 ' ' 1 । 1 । 1 1 ।... . । । । । । । । । 116 III 160173 208 | 1 rp! ■ 1‘* | ITT I | ■'I'r > | I I I I | I I I I | I I /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121837: Methane, dibromochloro- 129 — AAA— 4,80 5.00 5.20 5.40 5000 m/z 49.00 20.45%

208

Tl/Z-> .3, 6 4.74.9,. 20 40 60 -r-r-prM TTTPT 160173 80 100 120 140 160 180 200 220 240 al,........... 260 Abundance #57730: Methane, dibromochloro- 127 4.80 5.00 5.20 5.40 m/z 79.00 19.10%

5000

48 79 91 13 35 64 1114 — 160173 208 .A J IM . r1 1 1 1 1 f1 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 4.80 5.00 5.20 5.40

10986.D SCAN020507.M Thu May 16 09:23:00 2002 Page 4

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