Chain of custody record for GCMS analysis of sample AE10986 on May 22, 2002, including surrogate compound data.
NYC-WTC_000024450–000024462Folder label: “GCMS X 5/13/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LlDrary searen compouriu Keport
Data File : C:\MSDCHEM\1\DATA\020515\10986.D Vial: 16 Acq On : 16 May 2002 2:37 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
6.12 0.40 ug/1 29242 1,4 -Dichlorob'enzene-d4 11.38
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 36 23 Undecane, 5,7-dimethyl- 1H-Azonine, octahydro- 184 C13H28 127 C8H17N 017312-83-3 10 005661-71-2 9 4 2H-7\zepin-2-one , hexahydro-6-met.. . 127 C7H13NO 006142-55-8 9 Abundance / Scan 517 (6.117 min): 10986. D (-512) (-) m/z 43.10 100.00% 43
5000
' 1 ' I 1 1 1 1 I ' 1 ■ ■ i ' ' ' 'T 1 1 1 1 I 580 6.00 6.20 6.40 37 । ,A9...53.. df. ... 117 7 1‘1‘*‘II*‘‘IIISu1 1 ' ' I ' ' ' ' f 1 11 ' I 1 1 ‘ ‘ 1 1 1 ' 1 I 1 1 1 ’ I i I I | | | 1 i i | ' i'i'r | i i m/z 125.00 11.96% mlz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877:2-Propanone, 1,1,1-trichloro- 43
5000 ...........AA......... ‘ 1 ’ i ‘ ’ 1 ' i ' ■ ■ 11 1 1 1 T'1 ' > ' r 5.80 6.00 6.20 6.40 m/z 42.10 10.11% 27 36 .49 55 63 76 83 91 97 110117 125 -------- n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5598: Undecane, 5,7-dimethyl- 43 57 " ■'1 | ' r' ' | 17 । —49 r 5.80 6.00 6.20 6.40 5000 71 m/z 46.95 9.55% 85 29 — I 00 127 ...... 21.11,1381 913 1T nz->_______ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108185: 1H-Azonine, octahydro- ■ i ' ■ ■ ■ r 33 43 56 __ 5.80 6.00 6.20 6.40 ____________ m/z 84.00 9.14% 70 5000 84 96 127 MWMAykA.ws /z—> 15 "I "'I......... 1|h 10 20 30) -37440 +4494 50 63,11178,1,5, 90 J, 1034,112.12944, 6070 80 90 100 110 120 130 '■r1'1'1 ''i'11 ' ' i ' ' 1 ' i ■ ' ' ■ i ' ' ' 1 l ' ' ' ' I 5.80 6.00 6.20 6.40
10986.D SCAN020507.M Thu May 16 09:23:01 2002 Page 5
NYC-WTC_000024458
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000024472
Laboratory report documenting GCMS analysis of sample AE11152 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024730
Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024514
Laboratory report documenting GCMS analysis of sample AE11156 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024585
Laboratory report documenting GCMS analysis of sample AE11303 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024706
Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022575
Laboratory report of GCMS analysis for sample AE11481 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024770
Laboratory report of GCMS analysis for sample AE10241 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024915
Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022561
Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024596
Laboratory report documenting GCMS analysis of sample AE11304 conducted on May 28, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024681
Laboratory report documenting GCMS analysis of sample AE11159 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024463
Gas chromatography-mass spectrometry analysis of sample AE10987 completed May 22, 2002, showing unknown compounds and surrogate recovery at 89%.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000024423
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000024424
Brief log entry or header page from a GCMS analysis record dated between May 13 and May 16, 2002.
Filed in the same folder
NYC-WTC_000024427
Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.
Filed in the same folder
NYC-WTC_000024437
Laboratory report showing calibration results for volatile organic compounds using GCMS methods between May 13 and May 15, 2002.
Filed in the same folder
NYC-WTC_000024441
Laboratory record of reference standard analysis for volatile organic compounds using GCMS methods from May 13 to May 15, 2002.
Filed in the same folder