GCMS Method 508 scan results, April 2002

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' Data File : C: \MSDCHEM\1\DATA\020419\08487.D Vial: 24 Acq On : 20 Apr 2002 6:46 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Methane, oxybis[dichioro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.35 0.37 ug/1 489847 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, oxybis[dichloro­ 182 C2H2C140 020524-86-1 78 2 Methane, bromodi chloro­ 162 CHBrC12 000075-27-4 74 3 Methane, bromodi chi oro- 162 CHBrC12 000075-27-4 74 4 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 Abundance Scan 46 (3.349 min): 08487.D (-40) (-) m/ z 83.00 100.00% 83

5000

47 •==* 129 3.20 3.30 3.40 3.50 3.60 3.70 3.80 35 miz- > Of " I " " I " 111111,11 58.... , 93 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/ z 85.00 62.77% Abundance #33237: Methane, oxybis[dichloro- 83

5000 TTTTTTTTTMA 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z 47.05 19.38% 28

niz-> Ot ■ ■ I •' +.+,137.., 70 11 ,| 1 i ■ " ■ 11 ■ " i11111 ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 । " i ‘1" i " " 11" 11" " 11" ■ i " " i "

Abundance #116497: Methane, bromodichloro- 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 40.10 16.06%

47 28 129

miz-> Of TTp-- 1.37 1........ 1, I9,1, 11PPIPPWTTT II. "II" i■ i "i ■■"i" 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro-

w 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 48.10 14.07% 5000

47 129

m/z-> 0 .1103..20 27,335 .. 1163..72. 1’i’ 93 116 ||, 164 ■ I " " I ‘ 1 " I “ 114 1 1 I | I I I I | I n I | I ! > I | | | 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70 3.80

08487.D SCAN020418.M Mon Apr 29 08:36:46 2002 Page 19

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