GCMS results for sample AE09673, April 2002

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Data File : C:\HPCHEM\l\DATA\APR2502\9093.D Vial: 24 Acq On : 26 Apr 2002 2:43 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.81 1.09 ug/1 144241 Napht halene-d8 15.85 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 3,4-Dihydrox enzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 53 3 N- (Trifluoro cetyl)-0,OO''-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 Benzoic acid 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance ( Scan 1064 (14.811 min): 9093.D (-) m/ z 73.00 100.00%| 73

5000 267 355 —

45 14.40 14.60 14.80 15.00 15.20 103 133154 193 223 , i 323 ' l ' ■ i ■ '' ' i'f 1 '■ ' i1 ' 1 I ■ ' ■ > । ■ ’r । ■ ■ ■ ■ । । ■ ■ ■ । ■ m/z 355.05 43.82% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 42.91% ' i 1 ...... 207 I ,323, iz-> 50 100 150 200 250 300 350 400 450 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73 / IB 14.40 14.60 14.80 15.00 15.20 267 m/z 356.05 15.42%| 5000 179 356

m/z—> Abundance 50 44 45

100 147 ' ' I 1 1 1 1 1 1 —Ir It 150 200 209 237, 1 ■' 250 I1 | 1 1 312 ' I ■ ■ ■ 300 #58326: N-(TrifIuoroacetyl)-O,O',O"-tris(trimethylsilyl)no 1 i 350 1 1 1 1 I ' 1 1 400 1 I 450 1 '

73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 11.05%| 355 5000

45 | i. 126147 193 265 376 481 —- "ri m/z—> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00 15.20

9093.D GCMS0412.M Mon Apr 29 11:14:15 2002 Page 2

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