Laboratory report of GCMS re-injection analysis for sample AE09673 conducted on April 29, 2002.
NYC-WTC_000023778–000023788Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2502\9093.D Vial: 24 Acq On : 26 Apr 2002 2:43 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 17.97 0.51 ug/1 67008 Naphthalene-d8 15.85 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 50 2 Acetic acid, [bis[(trimethylsilyl)o 356 CllH29O5PSi3 053044-27-2 38 3 1,3,5,7,9/Pentaethylcyclopentasilox 370 C10H3005Si5 017995-44-7 23 4 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 16 Abundance Scan 1408 (17.969 min): 9093.D (-) m/ z 73.00 100.00% 73
341 5000
147 429 17.60 17.80 18.00 18.20
mfz—> 45 mmmmmp 117 | 179 207 i" “i 251 i" “I ■ ■" i1 ,-1' i 40 60 80 100120140160180200220240260280300320340360380400420 Ml " i" " r ■" r " ■ i ■ 11' i' m/z 341.00 52.19% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
5000 429 ■ i ■ ■ ■ ■ i ■ ■ L "I 17.60 17.80 18.00 18.20 7I"
m/z 429.15 19.52% 147 ill 1 117 |, 207 267 311 [ I_________ I 141—111110114841—10111801181041*9811890*142841480*2*8**84804**8**2*02** "'' i1 ■" । ■ i" " i";' i ■" ■ i ■ mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #49839: Acetic acid, [bis[(trimethylsilyl)oxy]phosphinyl]-, 73 341 ............. ............................ 17.60 17.80 18.00 18.20 5000 m/z 147.00 19.00% 251 297 133 211
mlz—> Abundance> 40 60 80 100120140160180 200 220240 260 280 300 320 340 360 380 400 42o ' #51267:1,3,5,7,9-Pentaethylcyclopentasiloxane 341 m 17.60 17.80 18.00 18.20 m/z 342.00 16.92% 87 5000 59 253 281 197 225 311 , ............................. I...... I...... i - 369 ............................... "’21111111111111111111111111111531111111 —031110011110111111037 '"I "■"i" "'[""I"" I1 m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 17.60 17.80 18.00 18.20
9093.D GCMS0412.M Mon Apr 29 11:14:15 2002 Page 3
NYC-WTC_000023785
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