NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2 502\30651.D Vial: 35
Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.27 5.10 ug/1 4429820 Naphthalene-d8 15.09
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36
2 l,l,l,5,7,7,7-HeptAmethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 27
3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
4 Silane, [1,2,3-bqnzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
Abundance Scan 1331 (17.266 min): 30651.D (-) m/ z 73.00 1 00.00%
73
5000
341
147
45 429 17.00 17.20 17.40 17.60
96 117 [ 397 179 . 207225 251
L 281 311 ( [
I , 0 I i
I ‘1" I TCIUIUCUammuuumaurWII0—0011——2310117 m/z 341.00 31.21%
m/z-> 40 60 80 100120140160180200220 240260280 300320340360380 400 420
Abundance #56711: Cyclohexasiloxane, dodecamethyl-
73
341
.................... ..............
429
5000
17.00 17.20 17.40 17.60
147 m/z 147.00 14.60%
117 1. 207 267 311
p •i." 11" " i" " i"r । p ’" p' .. ।.... ।. 11... । > 11 > ।. ■.. 11.. 1. i. ।. " "i ‘ ■" i ■" ■ i "■ ■ i11 ■ ■ I'
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #56714: 1.1.1,5.7.7,7-Heptametnyl-3.3-bis(trimetnvisijoxyit
73
147 17.00 17.20 17.40 17.60
5000 267 m/z 325.00 10.71%
355 429
45 207
|i
m/z-> "40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420
Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- -.......... —
73 341 17.00 17.20 17.40 17.60
m/z 342.00 10.56%
5000
45
91
.. .116 146........ 227... 269.... 3151
" " I ''.' I " '' | "I■ ।' 111 i'i 11 p i n | n n 111! 11 it I ! |! 11111 >'i 111 i 11111 n | iTi i f
I \
। 1 '1 ■ ।
miz-> 40 60 80 100120140160180200220240260 280 300 320 340 360 380 400 420 17.00 17.20 17.40 17.60
30651.D GCMS1126.M Mon Jan 28 12:23:16 2002 Page 4
NYC-WTC_000004224
OCR can misread numbers and units. Confirm readings against the page image before using them.