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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004224
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.27 5.10 ug/1 4429820 Naphthalene-d8 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 l,l,l,5,7,7,7-HeptAmethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 27 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1,2,3-bqnzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1331 (17.266 min): 30651.D (-) m/ z 73.00 1 00.00% 73

5000 341 147 45 429 17.00 17.20 17.40 17.60 96 117 [ 397 179 . 207225 251 L 281 311 ( [ I , 0 I i I ‘1" I TCIUIUCUammuuumaurWII0—0011——2310117 m/z 341.00 31.21% m/z-> 40 60 80 100120140160180200220 240260280 300320340360380 400 420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 .................... .............. 429 5000 17.00 17.20 17.40 17.60 147 m/z 147.00 14.60% 117 1. 207 267 311 p •i." 11" " i" " i"r । p ’" p' .. ।.... ।. 11... । > 11 > ।. ■.. 11.. 1. i. ।. " "i ‘ ■" i ■" ■ i "■ ■ i11 ■ ■ I' m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1.1.1,5.7.7,7-Heptametnyl-3.3-bis(trimetnvisijoxyit 73

147 17.00 17.20 17.40 17.60 5000 267 m/z 325.00 10.71% 355 429 45 207 |i

m/z-> "40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- -.......... — 73 341 17.00 17.20 17.40 17.60 m/z 342.00 10.56% 5000 45 91 .. .116 146........ 227... 269.... 3151 " " I ''.' I " '' | "I■ ।' 111 i'i 11 p i n | n n 111! 11 it I ! |! 11111 >'i 111 i 11111 n | iTi i f I \ । 1 '1 ■ । miz-> 40 60 80 100120140160180200220240260 280 300 320 340 360 380 400 420 17.00 17.20 17.40 17.60

30651.D GCMS1126.M Mon Jan 28 12:23:16 2002 Page 4

NYC-WTC_000004224

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NYC-WTC_000004224Source: NYC Law Department, mirrored locally

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