GCMS results for sample AE09019, April 30, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2502\9019.D Vial: 23 Acq On : 25 Apr 2002 12:13 pm Operator: Sample : re-inject Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD . R.T.

14.81 0.35 ug/1 50966 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 000541-02-6(91 370 C10H30O5S15 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 52 3 N-(Trifl roacetyl)-N,O,O’,0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Silane, /1 [4-[l,2-bis[(trimethylsily 458 C20H42O4Si4 056114-62-6 38 Abundance Scan 1064 (14.811 min): 9019.D (-) m/ z 73.00 100.00% 73

267 355 5000

45 14.40 14.60 14.80 15.00 15.20 — ——108 154 ,193.223 „ 323 ———— Tr TP—T ■ • i ■ ■ ■ ■ i ■ ' ■ ■ i ■ • ■ ■ i ' 1 m/z 355.05 54.44% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 53.53% ....................... 207 .i । 323, 1 ■ i' r miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3.4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73

14.40 14.60 14.80 15.00 15.20 5000 267 tn/z 356.05 24.43% 179 356

4 45 147 I, 209237, miz-> 50 100 11a _—.—.—J-

150 1di 200 250 300 4.312../%....... 350 400500 450 550 ■ ■ । • i

Abundance #60162: N-(TrifIuoroacetyI)-N,O,O',O“-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 15.20 m/z 357.05 14.84% 355 5000

45 1 t 1 11it । 147 193 267 538 ‘ । 1 ‘ | ‘ ‘ ‘ | ‘ ‘ ‘ | * 'r i’ r i ‘ ‘ ■ i ■ ' ■ 1 i ' ■ • ' i ■ ' ‘ ‘ i • • ■ ■ i ■ ‘ miz-s 50 100 150 200250300350400450500550 14.40 14.60 14.80 15.00 15.20

9019.D GCMS0412.M Fri Apr 26 11:07:52 2002 Page 2

NYC-WTC_000049439