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GCMS calibration table for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09518 analyzed in May 2002.

NYC-WTC_000023345–000023352

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0302\9518.D Vial: 19 ■ Acq On 4 May 2002 7:42 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.163 337 341 367 rVB 364393 862407 22.50% 4.415% 2 12.195 775 781 797 rVB 1179136 2738736 71.45% 14.021% 3 14.797 1059 1065 1072 rVB 94675 186535 4.87% 0.955% 4 15.823 1171 1177 1195 rBV 1676381 3494458 91.17% 17.890% 5 21.138 1750 1757 1771 rBV 1785072 3832839 100.00% 19.623% 6 23.273 1985 1990 1994 rVB 56187 109242 2.85% 0.559% 7 25.574 2234 2241 2250 rBV2 1672727 3569315 93.12% 18.274% 8 33.637 3114 3121 3136 rBV2 1172477 2614197 68.21% 13.384% 9 37.871 3574 3583 3598 rBV2 718609 2124856 55.44% 10.879%

Sum of corrected areas: 19532585 9518.D GCMS0501.M Tue May 07 09:38:12 2002

NYC-WTC_000023348

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NYC-WTC_000023348Source: NYC Law Department, mirrored locally

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