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GCMS calibration table for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.

NYC-WTC_000023363–000023371

Folder label: “GCMS X 5/8/02 A 5/9/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0302\9520 .D Vial: 21 Acq On 4 May 2002 9:41 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.167 336 341 371 rBV 2726248 6613803 100.00% 26.169% 2 9.954 532 536 552 rBV 29473 79996 1.21% 0.317% 3 12.190 775 780 796 rVB 1253133 2825918 42.73% 11.181% 4 14.792 1058 1064 1071 rVB 78476 155579 2.35% 0.616% 5 15.828 1171 1177 1193 rBV 1794112 3581609 54.15% 14.171%

6 21.134 1749 1756 1773 rBV 1913547 3942217 59.61% 15.598% 7 23.269 1982 1989 1994 rBV 77441 155140 2.35% 0.614% 8 25.578 2233 2241 2250 rBV2 1698100 3597384 54.39% 14.234% 9 33.633 3114 3120 3132 rBV2 1073973 2460483 37.20% 9.735% 10 37.866 3573 3582 3596 rBV2 636499 1861565 28.15% 7.366%

Sum of corrected areas: 25273694

9520.D GCMS0501.M Tue May 07 09:38:41 2002

NYC-WTC_000023366

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NYC-WTC_000023366Source: NYC Law Department, mirrored locally

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