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GCMS sample analysis summary, May 10, 2002

Machine-extracted title · confidence 90%

Summary of GC/MS analytical results for sample AE09675 processed on May 10, 2002, including surrogate recovery data.

NYC-WTC_000043600–000043608

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0602\9675.D Vial: 15 Acq On 7 May 2002 6:00 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.163 337 341 364 rBV 355915 814895 20.42% 4.212% 2 12.195 775 781 798 rVB 1235878 2837266 71.08% 14.665% 3 15.823 1171 1177 1193 rBV 1722432 3616670 90.61% 18.693% 4 21.138 1750 1757 1774 rBV 1855953 3991644 100.00% 20.632% 5 23.273 1983 1990 1996 rBV 184239 366573 9.18% 1.895%

6 25.573 2234 2241 2252 rBV2 1684809 3667671 91.88% 18.957% 7 33.637 3114 3121 3135 rBV2 1042399 2341706 58.67% 12.104% 8 37.862 3574 3582 3597 rBV2 580015 1710792 42.86% 8.843%

Sum of corrected areas: 19347217

9675.D GCMS0501.M Wed May 08 11:53:18 2002

NYC-WTC_000043605

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NYC-WTC_000043605Source: NYC Law Department, mirrored locally

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