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GCMS sample analysis summary, May 10, 2002

Machine-extracted title · confidence 90%

Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.

NYC-WTC_000043590–000043599

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0602\9674.D Vial: 14 Acq On 7 May 2002 5:02 am Operator: Sample GC/MS SCAN 4/24 FB Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 369 rBV 373291 885029 19.95% 4.068% 2 12.194 775 781 795 rVB 1377888 3105849 70.02% 14.277% 3 15.832 1171 1178 1193 rBV 1850029 3958462 89.24% 18.196% 4 21.138 1749 1757 1776 rBV 2145993 4435604 100.00% 20.390% 5 23.273 1983 1990 1996 rBV 197361 392655 8.85% 1.805%

6 25.573 2232 2241 2252 rBV2 1842065 4105161 92.55% 18.871% 7 25.719 2252 2257 2266 rVB 15695 44538 1.00% 0.205% 8 33.637 3114 3121 3136 rBV2 1240827 2803246 63.20% 12.886% 9 37.861 3574 3582 3598 rBV2 672100 2023515 45.62% 9.302%

Sum of corrected areas: 21754059

9674.D GCMS0501.M Wed May 08 11:53:06 2002

NYC-WTC_000043595

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NYC-WTC_000043595Source: NYC Law Department, mirrored locally

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