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GCMS sample analysis summary, May 10, 2002

Machine-extracted title · confidence 90%

Summary of GC/MS analytical results for sample AE09652 processed on May 10, 2002, including surrogate recovery data.

NYC-WTC_000043572–000043580

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0602\9652.D Vial: 10 Acq On 7 May 2002 1:07 am Operator: Sample GC/MS SCAN 4/24 FB Inst : 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.160 336 340 373 rVB 337769 794108 18.59% 3.832% 2 12.192 774 780 797 rBV 1338239 3001311 70.27% 14.482% 3 15.829 1171 1177 1193 rBV 1841265 3811888 89.25% 18.393% 4 21.135 1749 1756 1774 rBV 2086735 4270920 100.00% 20.608% 5 23.270 1982 1989 1994 rBV 182159 353661 8.28% 1.707%

6 25.580 2234 2241 2251 rBV2 1813453 3940034 92.25% 19.012% 7 33.634 3113 3120 3138 rBV2 1213856 2672334 62.57% 12.895% 8 37.859 3573 3581 3604 rBV2 656417 1880077 44.02% 9.072%

Sum of corrected areas: 20724333

9652.D GCMS0501.M Wed May 08 11:52:16 2002

NYC-WTC_000043577

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NYC-WTC_000043577Source: NYC Law Department, mirrored locally

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