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GCMS calibration data for TCLP method, May 2002

Machine-extracted title · confidence 100%

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000023076–000023083

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0302\9571.D Vial: 45 . Acq On 5 May 2002 11:08 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 373 rVB 394149 892000 21.77% 4.315% 2 12.194 775 781 798 rBV 1282820 2934677 71.62% 14.197% 3 14.796 1059 1065 1071 rBV 99715 192168 4.69% 0.930% 4 15.823 1171 1177 1195 rBV 1743994 3711773 90.59% 17.956% 5 21.138 1750 1757 1778 rBV 1923210 4097337 100.00% 19.822%

6 23.273 1983 1990 1998 rVB 153516 306133 7.47% 1.481% 7 25.582 2234 2242 2253 rBV2 1705747 3793287 92.58% 18.351% 8 33.637 3114 3121 3140 rBV2 1197102 2711434 66.18% 13.117% 9 37.870 3575 3583 3605 rBV2 678069 2032303 49.60% 9.832%

Sum of corrected areas: 20671112 9571.D GCMS0501.M Tue May 07 15:00:37 2002

NYC-WTC_000023079

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NYC-WTC_000023079Source: NYC Law Department, mirrored locally

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