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GCMS calibration data for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

NYC-WTC_000023122–000023129

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C: \HPCHEM\1\DATA\MAY0302\9574.D Vial: 47 . Acq On 5 May 2002 1:05 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.163 337 341 346 rBV 427014 843905 21.27% 4.114% 2 12.195 775 781 799 rVB 1231973 2869629 72.33% 13.989% 3 14.797 1059 1065 1071 rBV 152417 290840 7.33% 1.418% 4 15.824 1171 1177 1195 rBV 1717600 3643980 91.85% 17.764% 5 21.129 1750 1756 1772 rBV 1818525 3967341 100.00% 19.341%

6 23.274 1982 1990 1997 rBV 156277 308062 7.76% 1.502% 7 25.583 2234 2242 2252 rBV2 1668237 3682947 92.83% 17.954% 8 33.638 3114 3121 3140 rBV2 1225943 2727169 68.74% 13.295% 9 37.871 3574 3583 3604 rBV2 730117 2179205 54.93% 10.623%

Sum of corrected areas: 20513078

9574.D GCMS0501.M Tue May 07 15:01:04 2002

NYC-WTC_000023125

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NYC-WTC_000023125Source: NYC Law Department, mirrored locally

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