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GCMS calibration table for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09578 analyzed in May 2002.

NYC-WTC_000023327–000023334

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0302\9578 .D Vial: 51 . Acq On 5 May 2002 5:01 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.160 336 340 346 rBV 807694 1568607 40.89% 7.693% 2 12.192 771 780 795 rBV 1235491 2762290 72.00% 13.547% 3 14.794 1058 1064 1070 rVB 190106 367038 9.57% 1.800% 4 15.830 1171 1177 1193 rVB 1643130 3478783 90.67% 17.061% 5 21.135 1749 1756 1772 rBV 1833866 3836567 100.00% 18.815% 6 23.270 1983 1989 1995 rVB 87170 175853 4.58% 0.862% 7 25.580 2234 2241 2252 rBV2 1634768 3553879 92.63% 17.429% 8 33.634 3112 3120 3139 rBV2 1196364 2615432 68.17% 12.827% 9 37.868 3573 3582 3599 rBV2 681491 2032146 52.97% 9.966%

Sum of corrected areas: 20390595 9578.D GCMS0501.M Tue May 07 15:01:58 2002

NYC-WTC_000023330

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NYC-WTC_000023330Source: NYC Law Department, mirrored locally

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