GCMS reference standard results for sample AE08430, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0902\REF2.D Vial: 5 Acq On 9 May 2002 6:14 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 10:14 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.20 152 462535 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1684981 40.00 ug/1 0.00 17) Acenaphthene-diO 21.13 164 918107 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1296538 40.00 ug/1 0.00 38) Chrysene-dl2 33.64 240 847047 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 532190 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.28 209 162080 35.49 ug/L 0.00 Spiked Amount 40.000 Recovery 88.73%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.83 74 125940 10.81 ug/1 100 3) bis(2-Chloroethyl)ether 11.58 93 238800 15.80 ug/1 97 4) 1,3-Dichlorobenzene 12.10 146 174453 12.17 ug/1 98 5) 1,4-Dichlorobenzene 12.23 146 185928 11.86 ug/1 99 6) 1,2-Dichlorobenzene 12.76 146 183647 13.46 ug/1 98 7) 2,21-oxybis(1-Chloropropan 13.07 45 490492 16.74 ug/1 99 8) N-Nitrosodi-n-propylamine 13.46 70 177332 16.43 ug/1 96 9) Hexachloroethane 13.60 117 46017 8.25 ug/1 98 11) Nitrobenzene 13.87 77 218055 15.94 ug/1 98 12) 1sophorone 14.52 82 506292 18.88 ug/1 99 13) bis(2-Chloroethoxy)methane 15.20 93 288541 16.61 ug/1 99 14) 1,2,4-Trichlorobenzene 15.72 180 157122 13.43 ug/1 99 15) Naphthalene 15.88 128 580193 16.73 ug/1 99 16) Hexachiorobutadiene 16.43 225 44599 8.24 ug/1 98 18) Hexachlorocyclopentadiene 18.63 237 14722 3.16 ug/1 97 19) 2-Chloronaphthalene 19.39 162 352876 17.59 ug/1 98 20) Dimethylphthalate 20.48 163 441496 17.48 ug/1 100 21) 2,6-Dinitrotoluene 20.69 165 87552 16.21 ug/1 98 2 2) Acenaphthylene 20.66 152 561647 15.71 ug/1 100 23) Acenaphthene 21.22 153 373465 17.53 ug/1 100 24) 2,4-Dinitrotoluene 21.87 165 100565 17.27 ug/1 92 25) Diethylphthalate 22.62 149 433053 19.15 ug/1 100 26) 4-Chlorophenylphenylether 22.77 204 185690 16.61 ug/1 98 27) Fluorene 22.74 166 407207 18.13 ug/1 99 29) Azobenzene 23.23 77 448648 16.02 ug/L 99 31) N-Nitrosodiphenylamine 23.16 168 149365 18.44 ug/1 97 32) 4-Bromophenylphenylether 24.24 248 105310 16.43 ug/1 96 33) Hexachlorobenzene 24.67 284 127562 17.41 ug/1 99 34) Phenanthrene 25.64 178 545617 17.54 ug/1 100

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0510.M Fri May 10 10:15:53 2002 Page 1

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