GCMS reference analysis results for sample AE10515, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\REFC1.D Vial: 36 Acq On : 12 May 2002 12:13 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 16 13:43 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 16 09:35:44 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.16 152 670504 40.00 ug/1 -0.03 10) Naphthalene-d8 15.79 136 2466265 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.10 164 1327695 40.00 ug/1 -0.04 30) Phenanthrene-diO 25.54 188 1884874 40.00 ug/1 -0.03 38) Chrysene-dl 2 33.62 240 1210600 40.00 ug/1 -0.02 44) Perylene-dl2 37.84 264 724392 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.24 209 51555 7.81 ug/L -0.03 Spiked Amount 10.000 Recovery 78.10%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.81 74 160075 9.48 ug/1 96 3) bis(2-Chloroethyl)ether 11.56 93 297645 13.59 ug/1 96 4) 1,3-Dichlorobenzene 12.06 146 257941 12.41 ug/1 98 5) 1,4-Dichlorobenzene 12.20 146 272121 11.97 ug/1 98 6) 1,2-Dichlorobenzene 12.72 146 258202 13.05 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.04 45 612983 14.43 ug/1 98 8) N-Nitrosodi-n-propylamine 13.43 70 214193 13.69 ug/1 97 9) Hexachloroethane 13.57 117 78922 9.76 ug/1 96 11) Nitrobenzene 13.84 77 267971 13.38 ug/1 97 12) Isophorone 14.48 82 611812 15.59 ug/1 98 13) bis(2-Chloroethoxy)methane 15.17 93 349259 13.74 ug/1 100 14) 1,2,4-Trichlorobenzene 15.68 180 214896 12.55 ug/1 99 15) Naphthalene 15.85 128 747274 14.73 ug/1 99 16) Hexachlorobutadiene 16.40 225 85972 10.85 ug/1 98 18) Hexachlorocyclopentadiene 18.59 237 29501 4.38 ug/1 99 19) 2-Chloronaphthalene 19.36 162 452067 15.59 ug/1 97 20) Dimethylphthalate 20.45 163 533302 14.60 ug/1 100 21) 2,6-Dinitrotoluene 20.67 165 99759 12.77 ug/1 93 2 2) Acenaphthylene 20.63 152 673140 13.02 ug/1 100 2 3) Acenaphthene 21.19 153 462850 15.02 ug/1 99 24) 2,4-Dinitrotoluene 21.83 165 111457 13.24 ug/1 92 25) Diethylphthalate 22.58 149 521611 15.95 ug/1 99 26) 4-Chlorophenylphenylether 22.74 204 234849 14.52 ug/1 98 27) Fluorene 22.71 166 502236 15.46 ug/1 100 29) Azobenzene 23.20 77 551099 13.61 ug/L 98 31) N-Nitrosodiphenylamine 23.12 168 153443m 13.03 ug/1 32) 4-Bromophenylphenylether 24.20 248 127857 13.72 ug/1 97 33) Hexachlorobenzene 24.63 284 153084 14.37 ug/1 98 3 4) Phenanthrene 25.61 178 668740 14.79 ug/1 99

(#) = qualifier out of range (m) = manual integration REFC1.D GCMS0510.M Thu May 16 13:44:19 2002 Page 1

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