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GCMS reference analysis results for sample AE10515, May 2002

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GCMS reference standard report for sample AE10515 showing quantified compound levels from May 20, 2002.

NYC-WTC_000045305–000045312

Folder label: “GCMS X 5/2/02 A 5/12/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY1002\REFC1.D Vial: 36 Acq On : 12 May 2002 12:13 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 16 13:43 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 16 09:35:44 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.74 178 615323 13.08 ug/1 100 3 6) Di-n-butylphthalate 27.52 149 855858 14.66 ug/1 99 3 7) Fluoranthene 29.24 202 640623 14.18 ug/1 97 3 9) Pyrene 29.91 202 661810 16.22 ug/1 93 40) Butylbenzylphthalate 32.05 149 293904 14.15 ug/1 97 41) Benzo(a)anthracene 33.55 228 442515 14.06 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.84 149 366674 13.31 ug/1 99 43) Chrysene 33.68 228 464871 14.80 ug/1 99 45) Di-n-Octylphthalate 35.58 149 453462 11.98 ug/1 # 99 46) Benzo(b)fluoranthene 36.66 252 346214 13.33 ug/1 98 47) Benzo(k)fluoranthene 36.72 252 383269 13.94 ug/1 99 48) Benzo(a)pyrene 37.64 252 253757 10.81 ug/1 98 49) Indeno(1,2,3-cd)pyrene 41.90 276 276874 12.42 ug/1 97 50) Dibenz(a,h)anthracene 41.97 278 228184 12.85 ug/1 97 51) Benzo(g,h,i)perylene 43.12 276 247622 13.89 ug/1 98

(#) = qualifier out of range (m) = manual integration REFCI.D GCMS0510.M Thu May 16 13:44:20 2002 Page 2

NYC-WTC_000045308

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NYC-WTC_000045308Source: NYC Law Department, mirrored locally

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