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GCMS calibration results for sample AE10851, May 2002

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Laboratory report displaying GCMS calibration results for sample AE10851 on May 15, 2002, including response factors for target compounds.

NYC-WTC_000024197–000024208

Folder label: “GCMS X 5/10/02 A 5/15/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY15O2\REF1.D Vial: 4 Acq On : 15 May 2002 5:00 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 17 9:26 2002 <Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.74 178 406019 16.26 ug/1 100 36) Di-n-butylphthalate 27.52 149 606845 19.59 ug/1 99 37) Fluoranthene 29.23 202 442629 18.46 ug/1 # 89 3 9) Pyrene 29.91 202 459923 20.90 ug/1 92 40) Butylbenzylphthalate 32.05 149 210669 18.81 ug/1 94 41) Benzo(a)anthracene 33.55 228 319898 18.85 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.83 149 262521 17.67 ug/1 # 95 43) Chrysene 33.68 228 339493 20.04 ug/1 99 45) Di-n-Octylphthalate 35.58 149 330587 16.36 ug/1 # 90 46) Benzo(b)fluoranthene 36.66 252 270424 19.51 ug/1 98 47) Benzo(k)fluoranthene 36.72 252 284026 19.36 ug/1 97 48) Benzo(a)pyrene 37.64 252 179670 14.34 ug/1 97 49) Indeno(1,2,3-cd)pyrene 41.90 276 201823 16.96 ug/1 98 50) Dibenz(a,h)anthracene 41.98 278 169775 17.91 ug/1 95 51) Benzo(g,h,i)perylene 43.12 276 176192 18.51 ug/1 93

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0510.M Fri May 17 09:29:17 2002 Page 2

NYC-WTC_000024204

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NYC-WTC_000024204Source: NYC Law Department, mirrored locally

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