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GCMS reference analysis results for sample AE10515, May 2002

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GCMS reference standard report for sample AE10515 showing quantified compound levels from May 20, 2002.

NYC-WTC_000045305–000045312

Folder label: “GCMS X 5/2/02 A 5/12/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\REFC2.D Vial: 37 Acq On : 12 May 2002 1:11 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 16 14:07 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 16 09:35:44 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.74 178 562211 11.96 ug/1 100 36) Di-n-butylphthalate 27.52 149 763796 13.10 ug/1 100 37) Fluoranthene 29.23 202 571500 12.66 ug/1 99 3 9) Pyrene 29.91 202 582491 15.48 ug/1 95 40) Butylbenzylphthalate 32.05 149 257052 13.42 ug/1 94 41) Benzo(a)anthracene 33.55 228 370727 12.77 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.83 149 301594 11.87 ug/1 99 43) Chrysene 33.68 228 384434 13.27 ug/1 99 45) Di-n-Octylphthalate 35.58 149 346403 9.95 ug/1 # 96 4 6) Benzo(b)fluoranthene 36.66 252 309710 12.96 ug/1 97 47) Benzo(k)fluoranthene 36.73 252 321997 12.73 ug/1 98 48) Benzo(a)pyrene 37.63 252 202248 9.37 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.89 276 219835 10.72 ug/1 96 50) Dibenz(a,h)anthracene 41.98 278 187817 11.49 ug/1 99 51) Benzo(g,h,i)perylene 43.11 276 202531 12.34 ug/1 98

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0510.M Thu May 16 14:45:58 2002 Page 2

NYC-WTC_000045311

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NYC-WTC_000045311Source: NYC Law Department, mirrored locally

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