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GCMS calibration table review, May 2002

Machine-extracted title · confidence 100%

Reviewed data file listing retention times and response factors for deuterated internal standards.

NYC-WTC_000022757–000022762

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 3 0 2\REFB1.D Vial: 28 Acq On 4 May 2002 6:30 pm Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 11:39 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.78 178 550726 16.73 ug/1 99 36) Di-n-butylphthalate 27.55 149 768996 17.99 ug/1 99 3 7) Fluoranthene 29.27 202 556717 17.82 ug/1 99 3 9) Pyrene 29.94 202 578800 19.31 ug/1 98 40) Butylbenzylphthalate 32.08 149 272345 16.93 ug/1 96 41) Benzo(a)anthracene 33.58 228 412318 17.68 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.86 149 432989 20.92 ug/1 99 43) Chrysene 33.71 228 425942 18.78 ug/1 99 45) Di-n-Octylphthalate 35.60 149 475225 13.82 ug/1 99 46) Benzo(b)fluoranthene 36.69 252 377314 17.79 ug/1 97 47) Benzo(k)fluoranthene 36.75 252 401139 18.27 ug/1 97 48) Benzo(a)pyrene 37.67 252 274452 14.05 ug/1 98 49) Indeno(1,2,3-cd)pyrene 41.94 276 304754 18.53 ug/1 97 5 0) Dibenz(a,h)anthracene 42.02 278 252082 19.39 ug/1 98 51) Benzo(g,h,i)perylene 43.17 276 258470 20.53 ug/1 99

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0501.M Tue May 07 11:43:59 2002 Page 2

NYC-WTC_000022758

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GCMS calibration analysis CAL40, May 2002 · Box DEP Box 18

NYC-WTC_000023014

Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.

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