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GCMS analysis results for sample AE09570, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09570 conducted on May 14, 2002.

NYC-WTC_000023017–000023022

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY0302\REFCl.D Vial: 40 Acq On 5 May 2002 6:14 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:29 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.77 178 543525 15.36 ug/1 99 36) Di-n-butylphthalate 27.55 149 777989 16.93 ug/1 99 37) Fluoranthene 29.26 202 558459 16.63 ug/1 99 3 9) Pyrene 29.94 202 578763 17.71 ug/1 95 40) Butylbenzylphthalate 32.08 149 283905 16.18 ug/1 98 41) Benzo(a)anthracene 33.58 228 436810 17.17 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.85 149 396715 17.57 ug/1 100 43) Chrysene 33.71 228 471113 19.05 ug/1 99 45) Di-n-Octylphthalate 35.60 149 543160 14.82 ug/1 100 46) Benzo(b)fluoranthene 36.69 252 358351 15.84 ug/1 99 47) Benzo(k)fluoranthene 36.75 252 414047 17.69 ug/1 99 48) Benzo(a)pyrene 37.67 252 303226 14.56 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.95 276 314586 17.95 ug/1 99 50) Dibenz(a,h)anthracene 42.02 278 253118 18.26 ug/1 100 51) Benzo(g,h,i)perylene 43.17 276 268508 20.01 ug/1 98

(#) = qualifier out of range (m) = manual integration REFCI.D GCMS0501.M Tue May 07 14:30:56 2002 Page 2

NYC-WTC_000023018

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NYC-WTC_000023018Source: NYC Law Department, mirrored locally

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Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.

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