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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/9/02
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GCMS analysis results for sample AE09570, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09570 conducted on May 14, 2002.

NYC-WTC_000023017–000023022

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY0302\REFC2.D Vial: 41 Acq On 5 May 2002 7:12 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:31 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.77 178 471763 14.88 ug/1 100 36) Di-n-butylphthalate 27.55 149 660014 16.04 ug/1 99 37) Fluoranthene 29.27 202 473676 15.75 ug/1 98 3 9) Pyrene 29.94 202 491252 17.40 ug/1 95 40) Butylbenzylphthalate 32.08 149 230939 15.24 ug/1 96 41) Benzo(a)anthracene 33.58 228 349300 15.90 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.86 149 307569 15.77 ug/1 100 43) Chrysene 33.71 228 364756 17.08 ug/1 99 45) Di-n-Octylphthalate 35.60 149 398342 12.66 ug/1 100 46) Benzo(b)fluoranthene 36.69 252 311838 16.06 ug/1 97 47) Benzo(k)fluoranthene 36.75 252 331104 16.48 ug/1 97 48) Benzo(a)pyrene 37.67 252 235078 13.15 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.94 276 240166 15.96 ug/1 99 50) Dibenz(a,h)anthracene 42.01 278 195816 16.45 ug/1 99 51) Benzo(g,h,i)perylene 43.16 276 203132 17.63 ug/1 99

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0501.M Tue May 07 14:32:29 2002 Page 2

NYC-WTC_000023021

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NYC-WTC_000023021Source: NYC Law Department, mirrored locally

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Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.

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