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GCMS calibration table review, May 2002

Machine-extracted title · confidence 100%

Reviewed data file listing retention times and response factors for deuterated internal standards.

NYC-WTC_000022757–000022762

Folder label: “GCMS X 5/8/02 A 5/10/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0302\REFB2.D Vial: 29 Acq On 4 May 2002 7:29 pm Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 11:44 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.77 178 508006 16.75 ug/1 100 36) Di-n-butylphthalate 27.55 149 707472 17.96 ug/1 100 37) Fluoranthene 29.26 202 511327 17.77 ug/1 99 3 9) Pyrene 29.94 202 528778 19.80 ug/1 96 40) Butylbenzylphthalate 32.08 149 246866 17.22 ug/1 98 41) Benzo(a)anthracene 33.58 228 361855 17.42 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.85 149 379224 20.56 ug/1 99 43) Chrysene 33.71 228 382033 18.91 ug/1 99 45) Di-n-Octylphthalate 35.60 149 400324 13.92 ug/1 # 98 46) Benzo(b)fluoranthene 36.69 252 285549 16.09 ug/1 99 47) Benzo(k)fluoranthene 36.75 252 323399 17.61 ug/1 98 4 8) Benzo(a)pyrene 37.67 252 230553 14.11 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.95 276 236688 17.21 ug/1 99 50) Dibenz(a,h)anthracene 42.02 278 194882 17.92 ug/1 99 51) Benzo(g,h,i)perylene 43.17 276 202244 19.21 ug/1 99

(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0501.M Tue May 07 11:45:50 2002 Page 2

NYC-WTC_000022761

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NYC-WTC_000022761Source: NYC Law Department, mirrored locally

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GCMS calibration analysis CAL40, May 2002 · Box DEP Box 18

NYC-WTC_000023014

Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.

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