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GCMS reference standard results for sample AE08430, May 2002

Machine-extracted title · confidence 90%

Reference standard analysis for GCMS testing of sample AE08430 dated May 9, 2002, reporting quality control spike recovery values.

NYC-WTC_000023220–000023227

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023226
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 9 0 2\REF2.D Vial: 5 Acq On 9 May 2002 6:14 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 10:14 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.78 178 505891 15.63 ug/1 100 36) Di-n-butylphthalate 27.55 149 717037 17.86 ug/1 100 3 7) Fluoranthene 29.27 202 525752 16.92 ug/1 97 3 9) Pyrene 29.94 202 544855 19.08 ug/1 97 40) Butylbenzylphthalate 32.07 149 252170 17.35 ug/1 97 41) Benzo(a)anthracene 33.59 228 379127 17.22 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.86 149 328778 17.06 ug/1 100 43) Chrysene 33.71 228 394238 17.93 ug/1 99 45) Di-n-Octylphthalate 35.60 149 416654 14.98 ug/1 # 97 4 6) Benzo(b)fluoranthene 36.68 252 290204 15.21 ug/1 98 47) Benzo(k)fluoranthene 36.76 252 344215 17.04 ug/1 97 48) Benzo(a)pyrene 37.66 252 221622 12.85 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.95 276 241792 14.76 ug/1 93 50) Dibenz(a,h)anthracene 42.02 278 204309 15.66 ug/1 100 51) Benzo(g,h,i)perylene 43.16 276 210688 16.08 ug/1 99

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0510.M Fri May 10 10:15:54 2002 Page 2

NYC-WTC_000023226

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NYC-WTC_000023226Source: NYC Law Department, mirrored locally

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