GCMS reference analysis results for sample AE09447, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0802\REF2.D Vial : 5 Acq On 8 May 2002 2:29 pm Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:31 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 423670 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1539517 40.00 ug/1 0.00 17) Acenaphthene-diO 21.14 164 843482 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1168873 40.00 ug/1 0.00 38) Chrysene-dl2 33.63 240 672935 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 396757 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 37515 8.94 ug/L 0.00 Spiked Amount 10.000 Recovery = 89.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.83 74 127859 11.98 ug/1 99 3) bis(2-Chloroethyl)ether 11.59 93 239469 17.30 ug/1 98 4) 1,3-Dichlorobenzene 12.09 146 171083 13.03 ug/1 97 5) 1,4-Dichlorobenzene 12.24 146 185732 12.93 ug/1 99 6) 1,2-Dichlorobenzene 12.75 146 185137 14.81 ug/1 97 7) 2,21-oxybis(1-Chloropropan 13.07 45 497381 18.54 ug/1 99 8) N-Nitroso-di-n-propylamine 13.46 70 179355 18.14 ug/1 99 9) Hexachloroethane 13.60 117 42544 8.33 ug/1 94 11) Nitrobenzene 13.87 77 220131 17.61 ug/1 100 12) Isophorone 14.52 82 506681 20.68 ug/1 97 13) bis(2-Chloroethoxy)methane 15.21 93 288721 18.19 ug/1 99 14) 1,2,4-Trichlorobenzene 15.71 180 156909 14.68 ug/1 99 15) Naphthalene 15.88 128 583372 18.42 ug/1 99 16) Hexachlorobutadiene 16.43 225 38292 7.74 ug/1 97 18) Hexachlorocyclopentadiene 18.62 237 14014 3.28 ug/1 99 19) 2-Chloronaphthalene 19.38 162 359713 19.52 ug/1 98 20) Dimethylphthalate 20.48 163 438919 18.92 ug/1 99 21) 2,6-Dinitrotoluene 20.70 165 86045 17.34 ug/1 95 22) Acenaphthylene 20.66 152 561793 17.11 ug/1 100 23) Acenaphthene 21.23 153 375364 19.18 ug/1 100 24) 2,4-Dinitrotoluene 21.86 165 99426 18.59 ug/1 96 25) Diethylphthalate 22.61 149 430880 20.73 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 185818 18.09 ug/1 99 27) Fluorene 22.75 166 407189 19.73 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.23 77 451389 17.54 ug/L 97 31) N-Nitrosodiphenylamine 23.16 168 149913 20.53 ug/1 93 32) 4-Bromophenyl-phenylether 24.23 248 103740 17.95 ug/1 99 33) Hexachlorobenzene 24.66 284 122066 18.48 ug/1 97 34) Phenanthrene 25.64 178 537773 19.17 ug/1 100

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0507.M Thu May 09 14:33:16 2002 Page 1

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