GCMS calibration results, sample AD31129, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN0902\CAL40.D Vial: 2 Acq On : 10 Jan 2002 9:37 am Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 9:13 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.54 152 726809 20.00 ug/1 0.00 10) Naphthalene-d8 15.14 136 2888363 20.00 ug/1 0.02 17) Acenaphthene-diO 20.40 164 1438410 20.00 ug/1 0.00 2 9) Phenanthrene-dl0 24.81 188 2124608 20.00 ug/1 0.00 38) Chrysene-dl2 32.85 240 1351504 20.00 ug/1 0.02 44) Perylene-dl2 36.91 264 768404 20.00 ug/1 0.02

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 1358849m 38.97 ug/1 3) bis(2-Chloroethyl)ether 10.98 93 2213769 39.31 ug/1 99 4) 1,3-Dichlorobenzene 11.43 146 2037176 40.47 ug/1 100 5) 1,4-Dichlorobenzene 11.57 146 2072070 40.85 ug/1 100 6) 1,2-Dichlorobenzene 12.09 146 1932732 41.26 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 12.43 45 3356851 40.07 ug/1 97 8) N-Nitroso-di-n-propylamine 12.83 70 1429344 40.67 ug/1 99 9) Hexachloroethane 12.91 117 854544 41.20 ug/1 96 11) Nitrobenzene 13.22 77 2158991 38.73 ug/1 99 12) Isophorone 13.87 82 3962423 39.83 ug/1 99 13) bis(2-Chloroethoxy)methane 14.56 93 2555111 39.66 ug/1 100 14) 1,2,4-Trichlorobenzene 15.03 180 1589679 40.42 ug/1 99 15) Naphthalene 15.19 128 5421011 41.00 ug/1 100 16) Hexachlorobutadiene 15.73 225 834269 41.93 ug/1 99 18) Hexachlorocyclopentadiene 17.91 237 474952 47.01 ug/1 97 19) 2-Chloronaphthalene 18.67 162 3055945 41.01 ug/1 99 20) Dimethylphthalate 19.80 163 3551381 40.66 ug/1 100 21) 2,6-Dinitrotoluene 20.01 165 845806 40.85 ug/1 99 22) Acenaphthylene 19.93 152 4512489 41.12 ug/1 100 23) Acenaphthene 20.50 153 3118220 41.37 ug/1 100 24) 2,4-Dinitrotoluene 21.18 165 1096677 41.38 ug/1 98 25) Diethylphthalate 21.94 149 3571500 41.22 ug/1 100 26) 4-Chlorophenyl-phenylether 22.05 204 1477903 42.06 ug/1 98 27) Fluorene 22.01 166 3257590 42.62 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.52 77 4040280 39.40 ug/L 98

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0103.M Wed Feb 06 09:14:58 2002 Page 1

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