GCMS calibration results for volatile organics, Jan 2002

NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) + Data File : C:\HPCHEM\1\DATA\JAN0902\CAL40.D Vial: 2 Acq on : 10 Jan 2002 9:37 am Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Misc = Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 5 16:23 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator] Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.54 152 726809 20.00 ug/l 0.00 10) Naphthalene-ds 15.14 136 2888363 20.00 ug/l 0.02 17) Acenaphthene-d10 20.40 164 1438410 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 2124608 20.00 ug/1 0.00 38) Chrysene-d12 32.85 240 1351504 20.00 ug/l 0.02 44) Perylene-d12 36.91 264 768404 20.00 ug/l 0.02 System Monitoring Compounds 37) 2,4-DDD 0.00 235 od 0.00 ug/ml Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 1362344m 39.07 ug/l 3) bis (2-Chloroethyl) ether 10.98 93 2213769 39.31 ug/l 99 4) 1,3-Dichlorobenzene 11.43 146 2037176 40.47 ug/1 100 5) 1,4-Dichlorobenzene 11.57 146 2072070 40.85 ug/l 100 6) 1,2-Dichlorobenzene 12.09 146 1932732 41.26 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 12.43 45 3356851 40.07 ug/l 97 8) N-Nitroso-di-n-propylamine 12.83 70 1429344 40.67 ug/l 99 9) Hexachloroethane 12.91 117 854544 41.20 ug/1 96 11) Nitrobenzene 13.22 77 2158991 38.73 ug/l 99 12) Isophorone 13.87 82 3962423 39.83 ug/l 99 13) bis(2-Chloroethoxy) methane 14.56 93 2555111 39.66 ug/l 100 14) 1,2,4-Trichlorobenzene 15.03 180 1589679 40.42 ug/l 99 15) Naphthalene 15.19 128 5421011 41.00 ug/l 100 16) Hexachlorobutadiene 15.73 225 834269 41.93 ug/1 99 18) Hexachlorocyclopentadiene 17.91 237 474952 47.01 ug/1 97 19) 2-Chloronaphthalene 18.67 162 3055945 41.01 ug/l 99 20) Dimethylphthalate 19.80 163 3551381 40.66 ug/1 100 21) 2,6-Dinitrotoluene 20.01 165 845806 40.85 ug/1 99 22) Acenaphthylene 19.93 152 4512489 41.12 ug/1 100 23) Acenaphthene 20.50 153 3118220 41.37 ug/1 100 24) 2,4-Dinitrotoluene 21.18 165 1096677 41.38 ug/1 98 25) Diethylphthalate 21.94 149 3571500 41.22 ug/1 100 26) 4-Chlorophenyl-phenylether 22.05 204 1477903 42.06 ug/1 98 27) Fluorene 22.01 166 3257590 42.62 ug/l 99 28) Azobenzen/ 1,2-Diphenylhyd 22.52 77° 4040280 39.40 ug/L 98 (#) = qualifier out of range (m) = manual integration CAL40.D GCMS0103.M Tue Feb 05 16:24:33 2002 Page 1 NYC-WTC_000016913