GCMS calibration results for sample AD31017, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN0 8 0 2\CAL4 0.D Vial: 2 Acq On 8 Jan 2002 11:24 am Operator: 209 GALOS Sample calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 9:00 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.53 152 712378 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 2829983 20.00 ug/1 0.00 17) Acenaphthene-diO 20.40 164 1443852 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2104791 20.00 ug/1 0.00 38) Chrysene-dl2 32.85 240 1312509 20.00 ug/1 0.02 44) Perylene-dl2 36.91 264 723509 20.00 ug/1 0.02

System Monitoring Compounds 37) 2,4-DDD 29.73 235 17694 0.73 ug/mL -0.34 Spiked Amount 5.000 Recovery = 14.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 1375970 40.26 ug/1 98 3) bis(2-Chloroethyl)ether 10.98 93 2180779 39.51 ug/1 99 4) 1,3-Dichlorobenzene 11.43 146 1989742 40.33 ug/1 100 5) 1,4-Dichlorobenzene 11.57 146 2023336 40.70 ug/1 99 6) 1,2-Dichlorobenzene 12.08 146 1880038 40.95 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.43 45 3340115 40.68 ug/1 99 8) N-Nitroso-di-n-propylamine 12.83 70 1444790 41.94 ug/1 99 9) Hexachloroethane 12.91 117 844044 41.52 ug/1 95 11) Nitrobenzene 13.22 77 2169781 39.73 ug/1 99 12) Isophorone 13.86 82 3954450 40.57 ug/1 99 13) bis(2-Chloroethoxy)methane 14.56 93 2526457 40.02 ug/1 100 14) 1,2,4-Trichlorobenzene 15.03 180 1534158 39.82 ug/1 99 15) Naphthalene 15.19 128 5305095 40.95 ug/1 99 16) Hexachlorobutadiene 15.73 225 798332 40.95 ug/1 100 18) Hexachlorocyclopentadiene 17.91 237 405469 39.98 ug/1 99 19) 2-Chloronaphthalene 18.67 162 3009780 40.24 ug/1 98 20) Dimethylphthalate 19.80 163 3540330 40.38 ug/1 100 21) 2,6-Dinitrotoluene 20.01 165 859444 41.35 ug/1 99 22) Acenaphthylene 19.93 152 4547224 41.28 ug/1 100 2 3) Acenaphthene 20.50 153 3108779 41.09 ug/1 99 24) 2,4-Dinitrotoluene 21.18 165 1115640 41.93 ug/1 98 25) Diethylphthalate 21.94 149 3622527 41.65 ug/1 99 26) 4-Chlorophenyl-phenylether 22.05 204 1485956 42.13 ug/1 99 27) Fluorene 22.01 166 3228327 42.08 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.52 77 4128032 40.10 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Wed Jan 09 09:01:13 2002 Page 1

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