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GCMS calibration results for sample AD31017, Jan 2002

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Laboratory report documenting GCMS calibration analysis of sample AD31017 conducted on January 8, 2002, listing concentrations of various organic compounds.

NYC-WTC_000017334–000017337

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANO 8 02\CAL40.D Vial: 2 Acq On 8 Jan 2002 11:24 am Operator: 209 GALOS Sample calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 9:00 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.45 168 1324394 38.39 ug/1 99 31) 4-Bromophenyl-phenylether 23.50 248 792881 40.45 ug/1 95 32) Hexachlorobenzene 23.92 284 899432 39.64 ug/1 97 3 3) Phenanthrene 24.89 178 4317688 40.47 ug/1 99 34) Anthracene 25.02 178 4371361 41.88 ug/1 99 35) Di-n-butylphthalate 26.84 149 6020253 41.65 ug/1 100 36) Fluoranthene 28.49 202 4342056 42.42 ug/1 100 3 9) Pyrene 29.16 202 4409917 37.81 ug/1 99 40) Butylbenzylphthalate 31.34 149 2395838 37.88 ug/1 98 41) Benzo(a)anthracene 32.80 228 2987193 40.65 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.14 149 2990359 34.93 ug/1 99 43) Chrysene 32.93 228 2894069 40.07 ug/1 99 45) Di-n-Octylphthalate 34.88 149 4305837 36.96 ug/1 99 46) Benzo(b)fluoranthene 35.87 252 2371606 39.59 ug/1 98 47) Benzo(k)fluoranthene 35.94 252 2456641 41.67 ug/1 97 4 8) Benzo(a)pyrene 36.75 252 2007723 42.78 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.50 276 1835044 41.38 ug/1 99 50) Dibenz(a,h)anthracene 40.56 278 1396066 41.04 ug/1 99 51) Benzo(g,h,i)perylene 41.57 276 1467850m 39.66 ug/1

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Wed Jan 09 09:01:16 2002 Page 2

NYC-WTC_0000 17336

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NYC-WTC_000017336Source: NYC Law Department, mirrored locally

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