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← Document results/DEP Box 16/GCMS X 12/24/01 A 1/9/02 2/15/02
Document / 4 pages

GCMS calibration results, DEP Labs, Jan-Feb 2002

Machine-extracted title · confidence 100%

Analytical results for volatile organic compounds including nitrosamines and chlorinated benzenes.

NYC-WTC_000016366–000016369

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN0 8 0 2\CAL4 0A.D Vial: 2 Acq On 9 Jan 2002 2:43 pm Operator: 209 GALOS Sample calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 10:48 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.45 168 1250803 38.87 ug/1 97 31) 4-Bromophenyl-phenylether 23.50 248 744182 40.70 ug/1 97 32) Hexachlorobenzene 23.92 284 862486 40.74 ug/1 97 3 3) Phenanthrene 24.89 178 4052952 40.72 ug/1 99 34) Anthracene 25.02 178 4057306 41.67 ug/1 100 35) Di-n-butylphthalate 26.84 149 5608307 41.59 ug/1 100 36) Fluoranthene 28.49 202 4048100 42.39 ug/1 100 3 9) Pyrene 29.16 202 4109617 36.81 ug/1 99 40) Butylbenzylphthalate 31.35 149 2206578 36.46 ug/1 97 41) Benzo(a)anthracene 32.80 228 2823121 40.14 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.14 149 2739011 33.43 ug/1 99 43) Chrysene 32.93 228 2750991 39.79 ug/1 99 45) Di-n-Octylphthalate 34.88 149 3920848 34.52 ug/1 # 99 46) Benzo(b)fluoranthene 35.88 252 2242236 38.39 ug/1 99 47) Benzo(k)fluoranthene 35.95 252 2456996 42.74 ug'/l 99 4 8) Benzo(a)pyrene 36.75 252 1955115 42.72 ug/1 100 4 9) Indeno(1,2,3-cd)pyrene 40.50 276 1866288 43.16 ug/1 99 50) Dibenz(a,h)anthracene 40.56 278 1436999 43.33 ug/1 99 51) Benzo(g,h,i)perylene 41.57 276 1508047m 41.79 ug/1

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0103.M Wed Feb 06 10:49:17 2002 Page 2

NYC-WTC_0000 16368

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NYC-WTC_000016368Source: NYC Law Department, mirrored locally

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GCMS calibration results · Box DEP Box 16

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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