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GCMS calibration results, sample AD31129, Jan 2002

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GCMS calibration report for sample AD31129 listing response factors and concentrations for multiple organic compounds from January 10, 2002.

NYC-WTC_000018941–000018944

Folder label: “GCMS X 12/21/01 A 1/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN0902\CAL40 .D Vial: 2 Acq On : 10 Jan 2002 9:37 am Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 9:13 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.45 168 1351554 38.81 ug/1 97 31) 4-Bromophenyl-phenylether 23.50 248 787296 39.79 ug/1 97 3 2) Hexachlorobenzene 23.92 284 916417 40.01 ug/1 98 3 3) Phenanthrene 24.89 178 4393142 40.79 ug/1 99 34) Anthracene 25.02 178 4370086 41.48 ug/1 100 35) Di-n-butylphthalate 26.84 149 6002732 41.14 ug/1 100 36) Fluoranthene 28.49 202 4395720 42.54 ug/1 100 39) Pyrene 29.16 202 4456791 37.11 ug/1 99 40) Butylbenzylphthalate 31.34 149 2356464 36.19 ug/1 98 41) Benzo(a)anthracene 32.80 228 3093821 40.89 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.14 149 2872288 32.58 ug/1 99 43) Chrysene 32.93 228 3014645 40.53 ug/1 100 45) Di-n-Octylphthalate 34.88 149 4132204 . 33.40 ug/1 # 99 46) Benzo(b)fluoranthene 35.88 252 2411666 37.91 ug/1 99 47) Benzo(k)fluoranthene 35.95 252 2291100 36.59 ug/1 99 4 8) Benzo(a)pyrene 36.75 252 2081971 41.77 ug/1 99 49) Indeno(1,2,3-cd)pyrene 40.50 276 2047623 43.47 ug/1 99 50) Dibenz(a,h)anthracene 40.56 278 1578617 43.70 ug/1 99 51) Benzo(g,h,i)perylene 41.57 276 1626211 41.37 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0103.M Wed Feb 06 09:15:01 2002 Page 2

NYC-WTC_0000 18943

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GCMS calibration results · Box DEP Box 16

NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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