GCMS calibration results, DEP Labs, Jan-Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANO 8 02\CAL40A.D Vial: 2 Acq On 9 Jan 2002 2:43 pm Operator: 209 GALOS Sample calib mix • Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 10:48 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.54 152 696799 20.00 ug/1 0.00 10) Naphthalene-d8 15.14 136 2706141 20.00 ug/1 0.02 17) Acenaphthene-diO 20.40 164 1343113 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 1963542 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1256138 20.00 ug/1 0.00 44) Perylene-d12 36.91 264 705460 20.00 ug/1 0.02

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0d 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 1312514 39.26 ug/1 98 3) bis(2-Chloroethyl)ether 10.98 93 2105591 39.00 ug/1 99 4) 1,3-Dichlorobenzene 11.43 146 1938197 40.16 ug/1 100 5) 1,4-Dichlorobenzene 11.57 146 1966102 40.43 ug/1 100 6) 1,2-Dichlorobenzene 12.09 146 1825944 40.66 ug/1 98 7) 2,2’-oxybis(1-Chioropropan 12.43 45 3193967 39.77 ug/1 97 8) N-Nitroso-di-n-propylamine 12.83 70 1346313 39.96 ug/1 100 9) Hexachloroethane 12.91 117 807331 40.60 ug/1 97 11) Nitrobenzene 13.22 77 2047854 39.21 ug/1 99 12) 1sophorone 13.86 82 3730338 40.03 ug/1 99 13) bis(2-Chloroethoxy)methane 14.56 93 2414497 40.00 ug/1 100 14) 1,2,4-Trichlorobenzene 15.03 180 1492819 40.52 ug/1 99 15) Naphthalene 15.19 128 5079925 41.00 ug/1 100 16) Hexachlorobutadiene 15.73 225 786220 42.18 ug/1 99 18) Hexachlorocyclopentadiene 17.91 237 407119 43.15 ug/1 99 19) 2-Chloronaphthalene 18.67 162 2863375 41.15 ug/1 99 20) Dimethylphthalate 19.80 163 3333685 40.87 ug/1 99 21) 2,6-Dinitrotoluene 20.01 165 788124 40.76 ug/1 99 22) Acenaphthylene 19.93 152 4292838 41.89 ug/1 100 2 3) Acenaphthene 20.50 153 2930299 41.64 ug/1 99 24) 2,4-Dinitrotoluene 21.18 165 1023637 41.36 ug/1 99 25) Diethylphthalate 21.94 149 3343753 41.33 ug/1 100 26) 4-Chlorophenyl-phenylether 22.05 204 1381470 42.10 ug/1 99 27) Fluorene 22.01 166 3049041 42.72 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 22.52 77 3805073 39.74 ug/L 98

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0103.M Wed Feb 06 10:49:14 2002 Page 1

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