GCMS results for unknowns, sample AD30606, Feb 2002

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GCMS analysis report for sample AD30606 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000018858–000018869

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU-1\209\DATA\DEC2101\30606.D Vial: 19 Acq On : 23 Dec 2001 2:19 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************** * ************** Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.11 0.34 ug/1 141707 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -d10- 188 C14D10 001719-06-8 74 2 Phenanthrene/diO 188 C14D10 001517-22-2 64 3 5-Methyl-2-rahenyl-2-hexenal 188 C13H160 021834-92-4 43 4 Antipyrine / 188 C11H12N2O 000060-80-0 28 Abundance Scan 2186 (25.115 mln): 30606.D (-) m/z 188.10 100.00% 118

5000 94 2 V . . । j . r. । t i . , । . . . . । i . . . ( 158 65 80 . TTTg 38 HJHtm’t HH 53 108 132 146 , 24.80 25.00 25.20 25.40 m/z 9 .95 20.50% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 24.80 25.00 25.20 25.40 m/z 18 .10 18.05% ................. ........................................................................................................... miz-> 30 40 50 60 70 80 90 100 110 120 ‘136' 140 '156' 160 170 180 190 '' Abundance #19958' Phenanthrene-d10 188

24.80 25.00 25.20 25.40 5000 m/z 15 .05 16.07%

66 80 94 160 mmmmmTpmmP miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69187: 5-Methyl-2-phenyl-2-hexenal ■ ■ i ■ ■ ■ • । • 11 • । ■ ■ ■ ■ t । • • • । 188 24.80 25.00 25.20 25.40 117 m/z 18 .10 13.11% 5000 104 132 145 173

mlz-> • I “ •»I “ ’»I “ • * I •' “ I' •1 ’ l * “ • I “ “ I ’ all,...I,7 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .. । <... l.... ।... I‘ 4‘ t i-[ n !» । । । । । । » । । i । t i i i । 24.80 25.00 25.20 25.40

30606.D GCMS1126.M Tue Jan 29 14:20:44 2002 Page 4

NYC-WTC_000018868

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