GCMS results for unknowns, sample AD30606, Feb 2002

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Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2101\30606.D Vial: 19 Acq On : 23 Dec 2001 2:19 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Butanol, 3,3’-oxybis- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

11.44 0.39 ug/1 130778 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butano , 3,3’ -oxybis- 162.C8H1803 054305-61-2 59 2 Ethane, 1 - ethoxy-1 -methoxy- 104 C5H12O2 010471-14-4 59 3 2-Propa ol. 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 50 4 Methane, diethoxy- 104 C5H1202 000462-95-3 47 Abundance Scan 696 (11.436 min): 30606.D (-) m/z 59.05 100.00% 59 45 5000 73 103 11.20 11*40 11*60 11.80 39. 86 — 11‘ . II .... I’l'r. 11 > H m/z 45.05 53.40%

N_ miz-> 20 30 40 50 60 70 80 90 100 iw" 126' 130 140 Abundance #12859:2-Butanol, 3,3‘-oxybis- 59

5000 31 45 103 1120 11'40 1160 1180 ‘

N m/z 103.05 33.28% — r-j-n-rh-th ........................ 134 miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #1926: Ethane. 1-ethoxy-1-methoxy- 59 45 11.20 11.40 11.60 11.80 5000 m/z 73.00 7.28% 73 89 27 * | i l • • | • 'p . . . | | | . , 103 ■ i • ' ■ 1 1 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy> 59 11.20 1140 11.60 1180 m/z 41.0 5.24% 5000 45 103 73 31 'l■‘'1 '■..।I.1 . । ... I | ... H 11 ......... ,,,,,,, 1...................... ........... MMMAMY 111111111 11 11 m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 * 140 11.20 11.40 11.60 11.80

30606.D GCMS1126.M Tue Jan 29 14:20:39 2002 Page 3

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