GCMS results for unknowns, sample AD30606, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2101\30606.D Vial: 19 Acq On : 23 Dec 2001 2:19 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.75 0.70 ug/1 234781 1,4-Dichlorobenzene-d4 11.67 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone 1,1,l-trichloro- 160 C3H3C130 000918-00-3 42 2 2-Propanone l, 1-dichloro- 126 C3H4C120 000513-88-2 9 3 2 -Heptanone 114 C7H14O 000110-43-0 4 4 9-Decen-2 -o; 154 C1OH180 035194-30-0 4 Abundance Scan 295 (7.755 min): 30606.D (-) m/ z 42.95 100.00% 43

5000

• 1 i ‘ 1 ■ 1 1 1 1 1 ' i 1 TTTI11111 ‘ 7.40 7.60 7.80 8.00

m/z-> 10 ■ • i • ■ ■ ■ i ■ 20 35 111 ,'1'111 30 40 ■ 49.5965 75 82, ... 97.,...... 117 125 m/z 124.8,5 7.93% 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 • 1 I • ■ ' ■ i ■ • i . i | n . i . । i 7.40 7.60 7.80 8.00 15 m/z 58. 5 7.54% 35 ,49 85 97 117 125 • ' i ' ‘ ' i ■ 11 ■ • i ■ ITauuTm—uauuemBTTgT miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368: 2-Propanone, 1,1-dichloro- 43 ■ i ■ ■ ■ ' i ■ ■ ■ ■ i ■ Pi MMAi i f 7.40 7.60 7.80 8.00 5000 m/z 96.95 6.02% 15 27 „ ! 37 49 * oBTa ***3*1**** 63 76 83 93 • • i» miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3018:2-Heptanone A 1*n—n0n//mnTT 43 7.40 7.60 7.80 8.00 m/z 126.9.0 5.61% 58 5000

27 71 85 99p I 114 —I—B—B—mmmg 1 I » I I I I I I I I I < »« I I I I i ‘ > • • i ■ । ' 11 1 1 1 1 1 1 TT m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

30606.D GCMS1126.M Tue Jan 29 14:20:34 2002 Page 2

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