GCMS results for unknowns, sample AD30485, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC2101\30485.D Vial: 23 Acq On : 23 Dec 2001 6:12 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.75 0.58 ug/1 171896 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 50 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 2 - Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 4 1-Octadecanol 270 C18H380 000112-92-5 9 Abundance Scan 295 (7.750 min): 30485.D (-) m/z 42.95 100.00% 43

5000

1 1 i 1 f 1 1 t • ■ • ■ i ‘ 1 11r73 r । ... ....................... 37 —1 49 63 83 97 11 119125 7.40 7.60 7.80 8.00 ’ 1****I**’*I’’’1- m/z 124.95 9.75% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43 5000 ■ ■ I • ‘ 1 ■ | • I ‘ । ■ > | > rr r| i 7.40 7.60 7.80 8.00 15 m/z 96.95 7.50% 35 ,49 85 97 117 125 1’11011010m090’p—tfuonnnp—u9t TI’r ' l1 • • • i •' ‘ ■ i • ■ • ■ i • ‘ ■ i • • miz-> 10 20 30 40 50 «) 70 80 90 100 110 120 130 Abundance #4732: N-Acetyl pyrrolidone 43 7.40 7.80’ 7.80 8.00 1 r | i > > > | i

5000 m/z 82.95 7.06% 99 127 30 56 69 86 112 1 “ i' • ■ ■ ir'1111 '11 ‘'1111 Tmmmmp **1**1’**I** miz-> Abundance 10 20 30 40

43 50 60 70 80 #4368:2-Propanone, 1,1-dichloro- 90 100 110 120 130 AMAAAAAaLeLAA 7.40 7.60 7.80 8.00 m/z 81.95 6.53% 5000

15

m/z—> 27 37 49 63 ■ * i1 ■ ■ • i ■'' ■ i ■ ■ • • i ■ i *'l'| 1*** । »'i 1* 10 20 30 40 50 60 70 76 83 80 93 90 100 110 120 130 .. W.. 7.40 7.60 7.80 8.00

30485.D GCMS1126.M Tue Jan 29 14:18:41 2002 Page 2

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