GCMS results for unknowns, sample AD30485, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2101\30485.D Vial: 23 Acq On : 23 Dec 2001 6:12 am Operator: 209 GALOS Sanpl e : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.36 0.32 ug/1 95165 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Propa: 1, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 4 2 -Butanol , 3,3’ -oxybis- 162 C8H18O3 054305-61-2 39 Abundance Scan 688 (11.358 min): 3O485.D(-) m/z 59.05 10C .00% 59

5000

39 1 । 45

85 । 73 103 _M 11.00 11.20 11.40 11.60 ’ • l '

N IP- TTT r' ' i ‘ • i ■ • ■ • i ■ 1 ■ ■ i ■ ■ • ■ i • ■ ■ ■ i ■ ■ m/z 45.05 55.64% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 ■ । ■ 45 73 11.00 11.20 11.40 11.60 31 m/z 103.05 35.66% 1 1 I ''' 1 PI । । । । i . । 1111 ■ ■ ■ i1 ।'. i j — i i j-1 r । ] . 11 — - r 130 1 ' i ■ ■ • ‘ i ■ ■ mz-> 30 40 50 I60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol 2-(2 -hydroxypropoxy)- 59 • i ■ • • ' i ■ • ■ ■ i • ■ ■ ■ i । 1 1 1 i 1 11.00 11.20 11.40 11.60

M 5000 m/z 73.00 32.79% 31 45 103

■ ' I ■ ' ' I ils, . I ■ I j . 75 89 ' ■ 1 p ' ■ ■ i ■ ■ ■ ' i • ■ • ' i ' 1 1 ■ p ■ ‘ ■ i ■ • m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233:2-Propanol, 1-(2-methoxypropoxy) r 59 11.00 11.20 11.40 11.60

NA m/z 41.00 25.60% 5000

31 45 104 ■ • i • -LH— • I .... p73. । । । .'I . > p ■ ■ ■ i 1 1 1 130 1 I 1 1 AAAM m/z-> 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60 1 ‘11

30485.D GCMS1126.M Tue Jan 29 14:18:46 2002 Page 3

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